GCMS analysis results for sample AD30252, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.

NYC-WTC_000017854–000017878

Folder label: “GCMS X 12/13/01 A 12/27/01”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\DEC2 701\30252.D Vial: 22 Acq On : 28 Dec 2001 9:31 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 3 2-Butanol, 3,3'-oxybis- Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

11.45 0.41 ug/1 137671 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butanol, 3,3’-oxybis- 162 C8H18O3 054305-61-2 64 2 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 56 3 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 53 4 2-Propanol, 1-[1-methyl-2-(2-propen 174 C9H18O3 055956-25-7 40 Abundance Scan 698 (11.449 mln): 30252.D (-) m/z 59.05 100.00%

MJ i $

5000 45 73 103 11.20 11.40 11.60 11.80

.N . 39, 88 . i r । i n i । i i i 11 1 >i • ’Il .. ’ M . ।.r Tr I"i" i ri i ।11 1 1 TIBBBmTtttnnt rn/z 45.00 48.24% m/z~> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859:2-Butanol, 3,3’-oxybis- 59

5000 31 45 11.20 11.40 11.60 11.80

N 103 m/z 103.05 34.71% ■ uji । i1 j 1 ri ri [' i i 134 11 r1^ i—OmTTTTTT 1 i ■ 1 1 ■ i • 1 ■ • i ‘ Wz-> __ 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance ;#9238:2-Propanol, 1-(2-methoxy-1 -methylethoxy 1- 59 A 11.20 11.40 11.60 11.80 5000 103 m/z 73.00 29.07% 45 73

AM 31 i ............ ... ... .........................J............................. ........................ 130 ! ’1+***1***’I’’’’I’’*’I***+1***’1++**1*1’’I’* U’A4n4 1 I I | 1 > 1 1 | 1 I I 1 | 1 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6086:1-Propanol, 2-(2-hydroxypropoxy)- 11.20 11.40 11.60 11.80 m/z 41.00 22.65%

miz-> 5000 31

........................... ii ■ i ■ ■ ■ ■ i111111,1 20 30 40 45

TIP to ' i ■ 75 50 60 ■ ■ ‘ i ‘ 70 80 89 • i ■ ‘ 90 100 103

' i ‘ ■ ■1)111444 I 1 I 110 120 130 140 _MA ' I I * I' I I l * * j i 'l I J I IIIIII—1 11.20 11.40 11.60 11.80

30252.D GCMS1126.M Wed Jan 02 10:42:14 2002 Page 3

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GCMS analysis results for sample AD30425, Jan 2002 · Box DEP Box 16

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.

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