GCMS analysis results sample AD29462, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD29462 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036480–000036490

Folder label: “GCMS X 12/5/01 A 12/12/01”

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Data File : C:\HPCHEM\1\DATA\DEC1201\29462.D Vial: 22 Acq On : 12 Dec 2001 11:28 pm Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. .EstConc Area Relative to ISTD R.T.

11.35 0.46 ug/1 109428 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Butanol, 3,3 ‘-oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1,1 ‘- [ (1-methyl-l,2-eth 192 C9H20O4 001638-16-0 38 4 1-Propanol, -(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 38 Abundance . Scan 687 (11.348 min): 29462.D (-) m/z 59.05 100.00% 59

45 5000 - 103 73 v 11.00 1120 11.40 11.60

mlz—> ■ । 20 > i ■ 30 - —lL—40 51 ITT 50 60 70 88 , ' i ■ • 1 ' i ' ' ' ■ i ' 1 ■ ■ i ■ ■ ' ■ i ' ' ■ ■ i ' ■ ' ' i ‘

80 90 100 110 120 130 140 m/z 44.95 53.30% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 K1 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05 38.92% ._____ 1 —TT ......................... ,......................... 130............ ■ i ' ■ ■ ' i ■ ■ ■ ' i ■ miz-> 20 30 40 50 . 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3,3'-oxybis- 59 —T ■ I ■ ' 11.00 11.20 11.40 11.60

...I 5000- 31 45 m/z 41.00. 28.15% 103

I । 134 . i . . > . i . . . . i . 1 . . i . . . . I . . . . i . . . . i . . . . i . . . . i . . . . i . . . . i . . < . । < . . . । . m/z-> 20__ 30 40 50 60 70 80 90 100 110 120 130 140 'Abundance #20630: 2-Propanol, 1,r-[(1-methyl-1,2-ethanediyl)bis(oxy) 59 11.00 11.20 11.40 11.60 m/z 73.00 27 76%

m/z-> 5000 31 45

■ l • ■ ■ > l ' ■ ■ । । i r. . । . 20 30 39 I 40 50 —4 I ' 1 ' ' I ''' 60 70 73 80 90 100 103 L 110 117 120 130 140 r-r-j 111 11.00 _11.20 ill T TT tII T—IIT T-r-r-p 11.40 11.60

29462.D GCMS1126.M Fri Dec 21 12:29:50 2001 Page 2

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GCMS analysis results sample AD29461, Jan 2002 · Box DEP Box 22

NYC-WTC_000036469

Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.

1 shared topics · Same agency, volume and box · similarity 0.999