GCMS analysis results sample AD29462, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1201\29462.D Vial: 22 Acq On : 12 Dec 2001 11:28 pm Operator: 209 GALOS Sample : gc/msscan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.28 ug/1 786734 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 entative ID MW MolForm CAS# Qual

I N-Ethyl formamide 73 C3H7NO 000627-45-2 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 1,3-Dio: plane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 1,3-Dio olane. 2-methyl- 88 C4H802 000497-26-7 5 Abundance Scan 279 (7.602 min): 29462.D (-) m/z 73.0,0 100.00% 73

5000 - 43 7.20 7.40 7.60 7.80 8.00 38 |, | 49 5.5, 67, । | 78 87 ............. 103...................... ■ i ■ • ■ ■ i • ■ ■ • i ■ ■ ■ » । i i . ■ । i'.r 'i * 1 i । | ' m/ z 43.0.0 27.15% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73

5000 58 7.20 7.40 7.60 7.80 8.00 44 m/z 44.9.5 9.54%

m/z-> 10 5 20 30 — 40 50 60 70 80 90 100 110 120 'Abundance #62932: Silane, tetramethyi- 73

7.20 7.40 7.60 7.80 8.00 5000- m/z 41.00 9.39%

45 15 53 59 88 ' ' i ' ' ' ■ i ' ' ' ' i ' 1 1 1 i ■ ■ ' 1 i ■ ' I ' ‘ ' I ' 1 ' 1 I 1 TII i i i > । ■ n->-|-nrrrp-r m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-tricbloro-2,2-dimet 73 7.20 7.40 7.60 7.80 8.00 m/z 7 0.9,5 6.45% 5000-

45

3611 I ' ' ' ' I ' ' ' ' I 1 ' 1 'I' 55 67, 1 1 1 rT . । . । . i| । 109 115 ■ l ■ ■ ■ ■ l • ■ ■ ■ l • ■ ■ ' I • ■ ■ ■ l • ■ —CII——BTTTPTT miz—> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

29462.D GCMS1126.M Fri Dec 21 12:29:45 2001 Page 1

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