GCMS sample analysis AD29455, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1OO1\29456.D Vial: 5 Acq On : 12 Dec 2001 3:39 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.61 3.51 ug/1 1046250 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW. Mol Form CAS# Qual

1 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 1,3-Dioxolane, 2 - (3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 5 Abundance Scan 279 (7.606 min): 29456. (-) m/ z 73.00 1 00.00% 73

5000 43 87 ............ 103................... 7.20 7.40 7.60 7.80 8.00 37.1 L , , 55 1 1 1 k 67, i | > • i • • • ■ i • 1 1 1 1 m/ z 43.0.0 26.93% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73

............ — 5000 7.80 8.00 | 58 7.20 7.40 7.60 44 m/ Z 41.00 9.81% 15 — m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62932: Silane, tetramethyl- 73

7.20 7.40 7.60 7.80 8.00 5000- m/z 44.9.5 9.60%

45 15 53 59 ......... 88................................. ' i 1 ■ ■ ■ । ■ ■ ■ * । > TTddnnnn.n T ' • 101, m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet ----------------------- j 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.38% 5000 45 36 H ■ । ■ • • • । ■ • ■ • । ■ ■ ■ ■ । ■ 55 • i ■ 1: 67. ■ i ■ > - ■ | ■ +— 109 115 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

29456.D GCMS1126.M Wed Dec 19 13:00:33 2001 Page 1

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