GCMS sample analysis AD29455, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1OO1\29456.D Vial: 5 Acq On 12 Dec 2001 3:39 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.33 1.32 ug/1 394421 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, -(2-methoxy-l-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol, ,3 ‘-oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol/ 1,1'-oxybis- 134 C6H14O3 000110-98-5 50 4 1-Propanof, 2 -(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 'Abundance Scan 685 (11.333 min): 29456.D (-) m/z 59.05 100.00% I 59

5000

39 II i 45

83 89 73

। 103 N 11.00 11.20 11.40 11.60 f ------------ TH r' ■ i ■ ' ' • i ■ ' ' ■ i ' 1 ■ ■ i ■ ■ ' ' i ' ■ ' ■ i ' ' ' ■ i ■ m/z 44.95 1.93 49.43%

NA m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1 -methylethoxy) 59

5000 I ' ' ' ' I ' ' ' ' I ' ' ' ' I 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05 34.23% i |i......................... 130............ ■ i • ■ ' ■ i ' ■ 1 • i 1 —P 1—m— । . 11 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3°-oxybis- 59

11.00 11.20 11.40 11.60 5000 31 m/z 73.00 28.87%

A 45 103

. I ■ i • • > • । ■ I I 134 ' I ' miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,1’-oxybis- 59 11.00 11.20 11.40 11.60 m/z 41.05 - 25.30% 31 5000 45 103

m/z-> ■ i ■ • ■ ■ i ■ ■ • ■ i ■ 20 30 40 ।i 50 -72--- (60___ 70 80 90 100 110 120 130 140 J 11.00 11.20 11.40 11.60 '

29456.D GCMS1126.M Wed Dec 19 13:00:38 2001 Page 2

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