Laboratory analysis report for sample AD29455 conducted on December 28, 2001, including surrogate recovery data.
NYC-WTC_000036289–000036299Folder label: “GCMS X 12/4/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC1001\29456.D vial: 5 Acq On : 12 Dec 2001 3:39 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-1-met Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
11.42 1.70 ug/1 508144 1,4-Dichlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Propanol, 1- (2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Butanol, 3,3' -oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1- -methoxypropoxy)- 148 C7H1603 013429-07-7 50 4 1-Propanol, 2-/(2-hydroxypropoxy) - 134 C6H14O3 _______ 000106-62-7 42 'Abundance Scan 694 (11.416 min): 29456.D (-) m/z 59.05 100.00% 5(9
5000- 45 73
83 89 103
130 11.00 MA l ■ ■■ ■ l • ■ 11.20 11.40 ] ■ ■ ■ ■ l • ' 11.60 11.80 • I ■ ■ • • I ■ ----- — m/ Z 45.0.0 47.47%
N miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1 -methylethoxy) 59
5000 103 45 11.00 11.20 11.40 11.60 11 80 73 31 m/z 103.00 35.11% ------ ........... ।.......... 130 , , , ' I ' ' ’ ' I ' ' ' ' I 1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3‘-oxybis- 59 TIu 11.00 11.20 11.40 11.60 11.80 5000 31 m/ Z 73.00 26.82%
VN 45 103 I
. ! .I I —..... .............. 1................. 134 m/z-> 20 30 40 50__ 60___ 70 80 90 100 110 120 130 140 Abundance #9233: 2-Propanol, 1-(2-methoxypropoxy)- 5(9 11.00 11.20 11.40 11.60 11.80 m/ z 41- 05 22.85% 5000-
31 45 | HI 1 • I■'■•i•■■'i 1 ' ' TIT ,..,.|l|-,! 73- --- -MP 104 130 1mno ' 1 I 1 1 ' ' 1 1 • ' ' 1 1 ’ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80
29456.D GCMS1126.M Wed Dec 19 13:00:42 2001 Page 3
NYC-WTC_000036298
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NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 1.000
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036267
Laboratory analysis report for sample AD29295 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 1.000
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036103
Laboratory report noting GCMS scan results for sample AD29189 with di-n-butylphthalate detected and low pH.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036325
Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036255
Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036469
Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036403
Laboratory report documenting GCMS analysis of sample AD29299 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036447
Laboratory report documenting GCMS analysis of sample AD29459 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036126
Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036199
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036200
Laboratory methodology table documenting sample extraction parameters, surrogate recovery rates, and quality control data for mass spectrometry analysis.
Filed in the same folder
NYC-WTC_000036201
Laboratory record documenting the extraction method parameters for sample AD29229 analyzed in December 2001.
Filed in the same folder
NYC-WTC_000036205
Calibration data for volatile organic compounds including nitrosamines and chlorinated solvents from December 2001.
Filed in the same folder
NYC-WTC_000036210
Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
Filed in the same folder