Laboratory analysis report for sample AD29295 conducted on December 28, 2001, including surrogate recovery data.
NYC-WTC_000036267–000036277Folder label: “GCMS X 12/4/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C: \HPCHEM\1\DATA\DEC10 01\29296.D Vial: 9 Acq On 12 Dec 2001 7:32 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
11.42 1.39 ug/1 397341 1,4-Dichlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Propanol, -(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 90 2 2-Propanol/ 1,1'-oxybis- 134 C6H14O3 000110-98-5 56 3 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 50 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 'Abundance Scan 695 (11.422 min): 29296.D (-) m/z 59.05 100.00% 59
5000
39L 51 45
85 73
— ■ i ■ ■ ■ ■ i ■ ■ > 130 103 .ML 11.00 11.20 11.40 11.60 11.80 ' I ' ' ' ' I ' TIT । —4'11 —4 100 110 120 130 140 ■ ( ■ • • • i ■ m/z 45.00 46.15% 20 30 40 50 60 70 80 90 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59
5000- T I 45 103 11.00 11.20 11.40 11.60 11.80 I 73 I 31 m/ z 103.00 32.48% | ........... ,.......... 130.... > i • ■ ■ ■ i ■ ■ ■ ■ i ' ' i ' ■ ’ ' i ' ' ' ' I 1 miz-s 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,1‘-oxybis- 59 11.00 11.20 11.40 11.60 11.80 31 5000 45 I m/ z 73.00 26.08% 103 89 ! ‘I : ■ i ■ • • ■ । i ; I., • i ■ • ■ • i ■ 72 ’ i ' ' • ' i ■ । ।
m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3'-oxybis- ) 59 11.00 11.20 11.40 11.60 11.80 m/ z 41.05 23.47% 5000 31 45 103
.1 ' i ■ ■ ' ' i ' 1 ■ ' i ' ' ' 1 i ‘ ' HIT ............. ..... .... TTT TTur । I । । । । TT TIT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80
29296.D GCMS1126.M Wed Dec 19 12:58:29 2001 Page 3
NYC-WTC_000036276
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NYC-WTC_000036289
Laboratory analysis report for sample AD29455 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 1.000
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036103
Laboratory report noting GCMS scan results for sample AD29189 with di-n-butylphthalate detected and low pH.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036447
Laboratory report documenting GCMS analysis of sample AD29459 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036380
Laboratory report documenting GCMS analysis of sample AD29297 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036126
Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036469
Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036325
Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036255
Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036360
Laboratory GCMS analysis report for sample AD29289 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036199
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036200
Laboratory methodology table documenting sample extraction parameters, surrogate recovery rates, and quality control data for mass spectrometry analysis.
Filed in the same folder
NYC-WTC_000036201
Laboratory record documenting the extraction method parameters for sample AD29229 analyzed in December 2001.
Filed in the same folder
NYC-WTC_000036205
Calibration data for volatile organic compounds including nitrosamines and chlorinated solvents from December 2001.
Filed in the same folder
NYC-WTC_000036210
Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
Filed in the same folder