GCMS sample analysis AD29456, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1201\29285.D Vial: 13 Acq On : 12 Dec 2001 2:42 pm Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.33 0.98 ug/1 285505 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, -(2-methoxy-l-methylet 148 C7H1603 020324-32-7 83 2 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 50 3 2 - Propanol , 1,1' -oxybis- 134 C6H14O3 000110-98-5 50 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 • 000106-62-7 45 Abundance 7 Scan 685 (11.334 min): 29285.D (-) m/z 59.05 100.00% i 59

5000

II 39 45

l'l 11I I I . I . -4— . . . — 73

tr — - 85 103

l • ■ ■ ' I ' • ■ ■ I ' ll I I - _M 11.00 m/ z 11.20 45.05 11.40 11.60 50.05% ‘ T

miz-> 20 30 40 50 60 TO 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy}- 59 V 5000 ■ •। 1 ' ' TIm । । । । ।। 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05 34.97% ■ —P-H ......... , ............................................... 130............. m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3°-oxybis- 59

11.00 11.20 11.40 11.60 m/ Z 73.00 28.17%

NA 5000 31 45 103 i I _________ . ■__________ i______ ■ i ' ' ■ ' । ' ■ ■ ' । ■ 1 ' ■ i ' ' • ■ i ■ • ■ ■ । ■ ..... -.... 134 m/z-> 2G 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,1'-oxybis- 59 11.00 11.20 11.40 11 60_____ m/ z 41.00 25.48%

A 31 5000 45

103 — — i 1 89 — H 72 I ' i ' ' ' ■ i ' ' ' ' i ' ' ' ' i TT Tro m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60

29285.D GCMS1126.M Fri Dec 28 15:21:21 2001 Page 2

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