GCMS analysis report sample AD29229, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1201\29229.D Vial: 12 Acq On : 12 Dec 2001 12:44 pm Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K. L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.41 2.50 ug/1 738053 1,4-Dichlorobenzene-d4 11.68

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Butanol, 3,3‘-oxybis- 162 C8H18O3 054305-61-2 64 3 i-Propanol, 2 - (2-hydroxypropoxy) - 134 C6H14O3 000106-62-7 59 -methyl- 4 2-Pentanol, 22-methyl 102 C6H140 000590-36-3 42 'Abundance 7 Scan 693 (11.409 min): 29229.D (-) m/z 59.05 100.00% 59

5000 45

39 il — 44 ■ • ■ 73

— 89 103

130 ...M r 11.00 11.20 11.40 11.60 11.80 - ■ TTTT i । । . m/z 45.05 47.83% m/z-> 20 30 40 50 60 70 80 10090110 120 130 140 (Abundance #9238: 2-Propanol, 1-(2-methoxy-1 -methylethoxy)- 59

5000- v 45 103 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.00 33.01% । 130 - T , , । I J, , । . PPnt • ■ i ■ ' • • i ' ■ ■ ■ i ' 1 ■ ■ i ■ ' ■ ■ i ' ■ ' ■ I 1 ' ■ ■ i ■ m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3‘-oxybis- 59 V • ' l 1 i ■ ' 11.00 11.20 11.40 11.60 11.80 5000 31 45 m/ z 73.00 28.30% I 103

m/z-> Abundance 20 . ■i■ <■ • । ■ 30 I 40 i , .. !.......... ........134. 50 60

59 70 80 90 100 110 #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 120 130 140

11.00 m/ Z 11.20 41 .05 V 11.40 LA 11.60 TtT 11.80 22.69% 5000 31 45 103 V miz-> .. 20 ..40 r.. 30 50 4 (60 75 89 ' I ' ‘ ' ' I ' ' ' ■ i ' ■ ■ ■ i ' ■ ' ' i 1 1 1 ' i ' ■ ' ■ i ■ ■ ' ■ i ■ ■ ■ ' i ' 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80

29229.D GCMS1126.M Fri Dec 28 15:28:02 2001 Page 3

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