GCMS analysis comments, sample AD29088, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC10 01\29088.D Vial: 27 Acq On : 11 Dec 2001 2:02 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.35 0.43 ug/1 109678 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- -methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Butanol, 3 ,3 ‘-oxybis- 162 C8H18O3 054305-61-2 64 3 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 4 2 -Propanol- 1-(2-ethoxypropoxy)- 162 C8H18O3 010143-32-5 40 Abundance Scan 687 (11.354 min): 29088.D (-) m/ z 59.05 .00% 10C____ 1 59 I

5000 45 103 73 TT

m/z~> 20 Ll 30 40 50 60 70 80 88..... ।................. 90 100 110 120 130 140 11.00 m/z 11.20 45.05 11.40 11.60 44.38% 'Abundance 7#9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05. 36.65% ........ ' j......... 130.... m/z-> 20 ...... 30 H 40 ■ i ■ • ■ 1 i . ‘

50 60 ■ i 1

70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3.3'-oxybis- 59

11.00 11.20 11.40 11.60

—N 5000 31 45 m/z 73.00 25.34% 103 I I — 134 ■ i • • > ■ l • m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59 11.00 11.20 11.40 11.60 ___ m/z 41.05 — 23.98% 5000 - 31 45 103

,1, • | ' i • ■ 75 ■ ■ i ■ ■ 89 ■ ■ • ■ i ■ ‘ ■ ■ i ■ i • • • ■ i ■ > ■ ' i ■ ■ • • i ■

m/z--> 20 30 40 50 (60 70 80 90 100 110 120 130 140 11.00 11 20 11.40 11.60

29088.D GCMS1126.M Wed Dec 12 15:52:22 2001 Page 2

NYC-WTC_000036017