GCMS analysis comments, sample AD29029, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1001\29029.D Vial: 34 Acq On 11 Dec 2001 8:52 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.34 0.66 ug/1 191745 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 90 2 2-Propanol, 1,1‘-oxybis- 134 C6H1403 000110-98-5 50 3 2-Butanol, ,3 ‘-oxybis- 162 C8H18O3 054305-61-2 50 4 2-Propanol, 1-(2-methoxypropoxy) - 148 C7H16O3 013429-07-7 50 'Abundance Scan 686 (11.344 min): 29029.D (-) m/z 59.05 100.00% 59 5000 - 45 103 73 I-1 11.00 11.20 11.40 11.60

m/z-> 20 -51 30 40 50 60 80 70 90 85 r-pr-r-r-r-j-r 100 110 TI——BTI— . A , ( 120 । 130 < j . > , > । . 130 140 m/ z 45.05 46.04% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 v 45 11.00 11.20 11.40 11.60 73 31 m/z 103.05 33.94% __________ T , TTT ‘ | T-TT . | . I —mm ........... ।.......... 130.... miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,1‘-oxybis- 59 TIIIIT T 11.00 11.20 11.40 11.60 31 5000 45 m/z 73.00 27.88%

NA i

103 89 i ' l . . 72 11’11111 ' i ' ' ' 1 i ' ' ' ' i ' ■ ■ ■ i ■ ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3'-oxybis- Til 59 11.00 11.20 1140 11.60 m/z 41.05 23.15%

m/z-> 5000 -

-- #— P

20 31

30 40 45

50 Hmm 60 70 ..... '....... 134 80 90 103

100 110 120 130 140 ATTATT NA 11.00 11.20 11.40 11.60 11

29029.D GCMS1126.M Wed Dec 12 15:50:38 2001 Page 2

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