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GCMS analysis results sample AD29299, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD29299 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036403–000036413

Folder label: “GCMS X 12/5/01 A 12/12/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC12O1\29299. D Vial: 29 Acq On 13 Dec 2001 5:18 am Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C : \DATABASE\NBS75K . L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-1-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.41 1.44 ug/1 441323 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-methoxy- l-methylet 148 C7H16O3 020324-32-7 90 2 2 -Propanol, 1 ,Z‘ -oxybis- 134 C6H1403 000110-98-5 50 3 2-Butanol, 3,3 ‘ -oxybis- 162 C8H18O3 054305-61-2 50 4 2-Propanol, /1-(2-methoxypropoxy) - 148 C7H1603 ______ 013429-07-7 50 /' Scan 694 (11.412 min): 29299.D(-) Abundance m/z 59.05 100.00% 59

m/z~> 5000-

20 > । • • ■ • । ■ 30 40 45

—ll ■50l ■ • 460 — 70T —89+ 73

80 90 100 103

110 ...................... 130............ 120 130 140 11.00 m/ z _N 11.20 45.00 11.40 11.60 11.80 47.32% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)-

5000

31 45 59

73 103 11.00 UA 11.20 m/z 103.00 11.40 11.60 11.80 35.75% ,_____ I ........... ; '....... 130.... ■ i ■ ■ ' ' I 1 1 ■ • i 1 —P miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087; 2-Propanol, 1,1‘-oxybis- 59 ' T1 1 11.00 11.20 11.40 11.60 11.80 31 5000- 45 m/ z 73.00 28.05% i I | 103

m/z—> Abundance 30 i i ' i ' ■ ■ 1 I 1 20 1 i ' • ' ' i ■ 40 50 60

59 72 ' i • 1 ' ■ ( ' 70 80 89

90 100 #12859: 2-Butanol, 3.3’-oxybis- 110 120 130 140 TBBmmumr 11.00 m/ z 11.20 41.05 ) V UA 11.40 11.60 11.80 23.93%

m/z-> 5000

- - TIt 20 30 40 50 31

(60 45

80 103

...................................... 134 70 90 100 110 120 130 140 —d 11.00 11.20 V A 11.40 11.60 11.80

29299.D . GCMS1126.M Fri Dec 21 12:22:09 2001 Page 3

NYC-WTC_000036412

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NYC-WTC_000036412Source: NYC Law Department, mirrored locally

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