GCMS analysis comments, sample AD29234, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29189.D Vial: 20 Acq On : 11 Dec 2001 5:15 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.42 1.07 ug/1 233859 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Propanol, 1,1’-oxybis- 134 C6H14O3 000110-98-5 56 3 2-Butanol, 3,3 ’ -oxybis- 162 C8H18O3 054305-61-2 50 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 Abundance Scan 695 (11.422 mln): 29189.D (-) m/z 59.05 1 0.00%

_.N. 59

5000 45 103 73

—3s. 4 ....... 130.... 11.00 11.20 11.40 11.60 11.80 m/z 45.05 43.55% miz-> Abundance

5000 20 30

31 40

45 50

59 60 70 #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)

73

1 1 I ' 1 1 1H TInt I 11 80 90 100

103 110 120 130 140

................... 4............. 130........ T .N T T T 11.00 11.20 11.40 11.60 11.80 m/z 103.00 ' 1 1 '

32.98%

miz-> 20 30 40 50 (60 70 80 90 100 110 120 130 7 140 Abundance #6087: 2-Propanol. 1,1-oxybis- 59 11.00 11.20 11.40 11.60 11.80 31 5000 45 m/z 73.00 24.62%

m/z-> Abundance 20 30 40 72 — TTTTTTIPTTTTTT 50 60 70

59 80 90 89

100 110 120 130 140 #12859:2-Butanol, 3,3-oxybis- 103

m/z .N 1 1 * ‘ ' 1 1’11 I T 11.00 11.20 11.40 11.60 11.80 41.05 T

23.48% 5000 31

miz-> 20 40 45

—PPPPT + ■ ■ I ■ । i'i tr 30 50 60 80 103

■ i ■ ■ ■ ■ i ■ • ■ ' i ■ ■ ■ ■ i ■1 • ■ i • ‘ 70 90 100 110 ■ i • • ■ ■ i ■ ■ ■ • i ■ 120 130 134 140 A . । A_ fP9 . । , , , ■ । 11.00 11.20 11.40 11.60 11.80 , TI

29189.D GCMS1126.M Fri Dec 14 16:07:45 2001 Page 3

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