GCMS analysis comments, sample AD29088, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\DEC1001\29088 . D Vial: 27 Acq On : 11 Dec 2001 2:02 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.44 0.59 ug/1 149740 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2/methoxy-l-methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol, 1,1-oxybis- 134 C6H14O3 000110-98-5 56 3 1-Propanol, 2/(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 4 2-Butanol,__3 £3 1 -oxybis-___________ 162 C8H18O3 054305-61-2 39

M Abundance Scan 696 (11.437 min): 29088.D (-) m/ z 59.05 100.00% 59

5000 - 45 103 73 11.20 11.40 11.60 11.80

m/z-> . —3430 40 50 14—। ——— I60 _______ 86 70 80 90 100 110 120 130 m/z 45.00 47.36% Abundance ■ #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy^ 59

5000 45 103 11.20 11.40 11.60 11.80 73 31 m/z 103.05 34.80% Ptt 80 90 100 1 110 130 m/z-> 30 40 50 60 70 120 130 Abundance #6087: 2-Propanol, 1,1-oxybis- 59 — '"'■'111 r 11.20 11.40 11.60 11.80 31 5000- 45 m/z 73.00 9.12%

—N 103 89 72 i 1 i ■ ■ ■ ' i ■ ■ ■ ■ i ' ■ ' ' i ■ ■ ' ' i ■ ' ' ■ i ' m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59 11.20 11.40 11.60 11.80 m/ 2 41.05 24.92% 5000 - / 31 45 103

1 I .758 ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ' ■ i ■ ■ ■ ' i • 1 ' ■ i ■ ' ■ ■ i • ■ ■ ■ I ■

mlz-> 30 40 50 I60 70 80 90 100 110 120 130 11.20 11.40 11.60 11.80

29088 .D GCMS1126.M Wed Dec 12 15:52:27 2001 Page 3

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