GCMS analysis report sample AD29229, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1201\29229.D Vial: 12 Acq On : 12 Dec 2001 12:44 pm Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise. Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Propanedioic acid, hexyl-, die Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

35.56 0.83 ug/1 150628 Perylene-d12 37.10

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 35 2 Benzene, 1-nitro-2 - (octyloxy) - 251 C14H21NO3 037682-29-4 32 3 1-Decene, 2,4-dimethyl- 168 C12H24 055170-80-4 25 4 2,4,6(AH,3H,5H)-Pyrimidinetrione, 5 240 C12H20N2O3 051209-91-7 16 Abundance Scan 3324 (35.563 min): 29229.D (-) m/z 185.10 100.00% 185 57 5000- 70 43 _ 112 83 98 I I J | 125 143 157 203 221 35.20 35.40 35.60 35.80 281 —Tt ■ ■ I ' ' 1 1 I' ■ ' ' I ' ' ' ' I ' ' ' ' I ' ' m/ z 57.00 59.80% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #32687: Propanedioic acid, hexyl-, diethyl ester 57 70

5000 *f 11 1 I...... TF 83 112 35.20 35.40 35.60 35.80

7_ 42 . 98 — | 199 217 r-p m/z--> . 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #34102: Benzene, 1-nitro-2-(octyloxy)- 57

71 35.20 35.40 35.60 35.80 5000- m/z 70.10 42.91% 83 112 139

-7 |........... 221.. 251... m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #14795: 1-Decene, 2,4-dimethyl- ----- T14 r 43 57 35.20 35.40 35.60 35.80 m/ Z 71.10 40.09% 83 5000 70 112

m/z—> • ■ i > • 40. 60 i ' ' '' । 80 97 100 ......... 168......................... 120 140 160 180 200 220 240 260 280 ■ i ■ ' • ■ l —AMA-— 35.20 35.40 35.60 35.80

29229.D GCMS1126.M Fri Dec 28 15:28:07 2001 Page 4

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