NYC-WTC_000035089
Laboratory report noting TurboVap contamination with recovery data for sample AD28693.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 18 pages
GCMS analysis comments for sample AD28694, Dec 2001
Machine-extracted title · confidence 100%Laboratory report noting di-n-butylphthalate detection and low pH with recovery data for sample AD28694.
NYC-WTC_000035135–000035152Folder label: “GCMS X 11/24/01 A 12/4/01”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC04 01\28694.D Vial: 5 Acq On 4 Dec 2001 4:16 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Decanedioic acid, bis(2-ethylh Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 35.59 6.56 ug/1 1341920 Perylene-d12 37.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 2 [1,1'-Biphenyl]-4-ol, 3-amino- 185 C12H11NO 001134-36-7 3 Butyl citrate 360 C18H3207 000077-94-1 32 4 2,4,6(1H,3H,5H)-Pyrimidinetrione, 5 240 C12H20N2O3 051209-93-9 25 Abundance Scan 3328 (35,594 min): 28694. D (-) m/z 185.10 100.00% 185
5000 57 70 43 , 1 112 114 J‘d LLi 1 83 98 125 143 166 35.20 35.40 35.60 35.80 36.00 203 268281 297 315 * Hr 4 r i 4 — , i । ■ । TT । ■ ■ • > । 11 ‘1 11 I’ m/z 57.00 48.44% mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185
5000 57 71 112 35.20 35.40 35,60 35.80 36 00 m/z 70.00 34.37% 4 98 125 143 166 203 298 316 ■ “ T TT I'1' • 11''1 11 1 TIITTTTTT TI0—011nannnuunutur m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #19199: [1,1‘-Biphenyl]4-ol, 3-amino- 185
35.20 35.40 35.60 35.80 36.00 5000 m/z70.95 32.97% 139 156
miz-> ... .. 113 4 60 80 40 T ।।111■।। ■ ■ ■ ■ । 100 120 140 160 180 200 220 240 260 280 300 320 । । ■ ■ ■ ■ । ■ 1111111111
Abundance #50331: Butyl citrate T 185 35.20 35.40 35.60 35.80 36.00 129 m/z 112.10 28.90% 5000
57 259 111
m/z—> ——l 100 120 140 160 180 200 220 240 260 280 300 320 40 60 80 , 143157 213 TTTTTTTTT TITTT_uI—C0—EITTTTOECTiT 35.20 35.40 35.60 35.80 36.00
28694.D GCMS1126.M Thu Dec 06 15:34:19 2001 Page 11
NYC-WTC_000035151
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