GCMS sample analysis AD29294, Dec 2001

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Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.

NYC-WTC_000036255–000036266

Folder label: “GCMS X 12/4/01 A 12/10/01”

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Data File : C:\HPCHEM\1\DATA\DEC1OO1\29295.D Vial 7 Acq On : 12 Dec 2001 5:35 am Operator 209 GALOS Sample : gc/ms scan 12/4 Inst GC/MS 209 Mise Multiplr 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

35.57 22.24 ug/1 4433250 Perylene-dl2 37.10

'Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis (2-ethylhexyl) 426 C26H50O4 000122-62-3 91 2 [1,11 -Biphenyl] -4-ol, 3-amino- 185 C12H11NO) 001134-36-7 35 3 Pyridine, 4- [4-methoxyphenyl] - 185 C12H11NO> 000000-00-0 17 4 Pyridine, 4- [4-methoxyphenyl] - 185 C12H11NO>____ 000000-00-0 17 •Abundance Scan 3325 (35.566 min): 29295.D (-) m/z 185.10 100.00% 185

57 5000 71 43 112 98 TT TT 35.20 35.40 35.60 35.80 111117 129143 .166 240254268 T TTT TTT TTTT II i l I 1 • ■ • 203 297 315 340 m/z 56.95 53.46% i TTT • i l * TTTT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185

5000 57 71 112 35.20 35.40 35.60 35.80 m/z 70.00 36.78%

L 98 143 166 298 316 ■ ■ ■ i • ■' 11 ■ XX T'1 1 1 I TTTT 203 ■ T'' 11 '''I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #19199: [ 1.1 '-Biphenyl ]-4-ol, 3-amino- 185 ■ ■ i ■ 35.20 35.40 35.60 35.80 5000- m/ Z 71.05 36.69%

-n-T-j-T-m-j-r ............ 113 139 156 | j TTTTPTPIIIITT II—rrr T I' ’' • I''' ’ I 1''' I ’'1 ’ 1 1 I ' ' ' ' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #19197: Pyridine, 4-[4-methoxyphenyl]- 185 35.20 35.40 35.60 35.80 m/z 112.10 31.00% 5000- 142 115 170 63 89 I । I T...... Ji...... I......... ............... . . . _ , _ .................. ' ' I ' " ' I' ' " I' '" I ' ' ' 11 ' ‘ ' I ' 1 T T1 ’ II"’1111TET TTTTTTTTTTttrrT - TTT ITT m/z-> 40 60 80 . 00 120 140 160 180 200 220 240 260 280 300 320 340 35.20 35.40 35.60 35.80

29295.D GCMS1126.M Wed Dec 19 12:57:20 2001 Page 4

NYC-WTC_000036265

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GCMS sample analysis AD29296, Dec 2001 · Box DEP Box 22

NYC-WTC_000036278

Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.

1 shared topics · Same agency, volume and box · similarity 0.999