GCMS calibration data for TCLP analysis, March 2002

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Technical record of GCMS calibration data for TCLP analysis using sample vial 12 from March 28, 2002.

NYC-WTC_000011934–000011941

Folder label: “GCMS X 2/28/02 A 3/26/02”

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Data File : C:\HPCHEM\1\DATA\MAR2502\4385.D Vial: 12 Acq On : 25 Mar 2002 9:03 pm Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

36.17 25.89 ug/1 1966640 Perylene-dl2 37.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 76. 2 [1,11-Biphenyl]-4-ol, 3-amino- 185 C12H11NO > 001134-36-7 38 3 Pyridine, 4-[4-methoxyphenyl]- 185 C12H11NO> 000000-00-0 17 4 Pyridine, 4-[4-methoxyphenyl]- 185 C12H11NO> _ 000000-00-0 17 Abundance Scan 3391 (36.173 min): 4385.D (-) m/ z 18 5.10 100.00% 185

5000 57 71 112 43 98 TT0129143 ’70’T11.166 35.80 36.00 36.20 36.40 36.60

m/z-> — 40 60.. 80 kkhrr [ 203 240 268282297 315 341 TTTT.m—mam—u——umTmmorr m/z 100 120 140 160 180 200 220 240 260 280 300 320 340 57.00 45.34% Abundance #55661: Decanedioic acid, bis(2-ethylhexy!) ester 185

5000 57 71 112 35.80 36.00 36.20 36.40 36.60 m/z 71.10 32.51% 98 203 143 , 298 316 - —1—I mmmPTT1 79 190 ■ ■ i ■ ■ ■ ■ i1 ■ ■ ■ i ■ ■' ■ i' ‘ “ i ■' ■ ■ i' " 11 • • “ i' ■ m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance — 00 •: 1 ' a ■ 185

35.80 36.00 36.20 36.40 36.60 5000 m/z 70.10 32.14% 139 156 113 -TT-p-TT-rp- 1******* P *«1 p 1 < * P * * 11 > > *«i * *' • । < < * * । * * • ■ । ■ * * * । < * < • । ■ < * । j * • m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #19197: Pyridine, 4-[4-methoxypheny!]- 185 35.80 36.00 36.20 36.40 36.60 m/z 112.10 27.16% 5000 142 115 170 63 89 I J I Jl m/z-> 40 60 80 100 ‘120 140 160 180 200 ‘220 240 260 280 300 320 340 35.80 36.00 36.20 36.40 36.60

4385.D GCMS0308.M Thu Mar 28 12:28:57 2002 Page 2

NYC-WTC_000011940

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GCMS calibration table for TCLP analysis, March 2002 · Box DEP Box 14

NYC-WTC_000011949

Technical record of GCMS calibration data for TCLP analysis using sample vial 14 from March 28, 2002.

1 shared topics · Same agency, volume and box · similarity 0.998