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GCMS analysis results for sample AE04943, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE04943 conducted on April 5, 2002.

NYC-WTC_000058668–000058677

Folder label: “GCMS X 3/6/02 A 3/30/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR3OO2\4943.D Vial:. 10 Acq On : 29 Mar 2002 11:53 pm Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

36.18 2.02 ug/1 138734 Perylene-dl2 37.93

Hit# of 5 Tentative ID MW MolForm CAS# Qua!

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3^;P^ 2 Butyl citrate 360 C18H32O7 000077-94-1 32 3 Pyridine, 4-[4-methoxyphenyl ]- 185 C12H11NO 000000-00-0 25 4 Carbamic acid. (4-chlorophenyl)-, m 185 C8H8C1NO2 000940-36-3 9 Abundance Scan 3391 (36.178 min): 4943.D (-) m/z 185 . in.... lodTo0% If ;5

5000 sr ,0 43 112

■m/z-> Abundance UI4. 40 60 83

80 1 125139 166 203 ' I ' ' ' ' I 100.. 120 140 160 180 200 220 240 260 280 300 320 #55661: Decanedioic acid, bis(2-ethylhexyl) ester 253 268281 297 315 35.80 36.00 36.20 36.40 36.60 m/z”'57". 00 36.52% ' ' I '

185

57 ............... ,,,/, ............ .. 5000 71 112 35.80 36.00 36.20 36.40 36.60 m/z 30.95% . iT. 166 ii 203 T-a-r I ‘ ‘ ' I 298 316 Y-TT-r-iYr-r-r-l-p- rn/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #50331: But/citrate 185 129 35.80 36.00 36.20 36.40 36.60 5000 m/ z '7^ • 91° 28.13% I 57 259 1 87 111 143^57

Ik I rp-r-n-p 213 I' '''I''' 'I I ' ' ‘ ' I ' ' ' ' I I ' ' ' ' I ' m/z-> ±0__60__ 80 100 120 140 160 180 200 220 240 260 280 300..320 Abundance #19196: Pyridine, 4-[4-methoxyphenyl]- 1*5 35;8^0 36,00 36;20 3640 36^ m/z 55.00 24.99% 5000 142 115 170 6,3 89

m/z-> ....60.......... 40 I,,,,,;., I 80 100 120 140 160 180 200 220 240 260 280 300 3201 35.80 36.00 36.20 36.40 36.60

4943.D GCMS0308.M Tue Apr 02 11:07:00 2002 Page 2

NYC-WTC_000058676

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NYC-WTC_000058676Source: NYC Law Department, mirrored locally

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