GCMS analysis results for sample AE04943, April 2002

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Data File C:\HPCHEM\l\DATA\MAR3002\4943.D Vial: 10 Acq On 29 Mar 2002 11:53 pm Operator: Sample gc/ms scan 3/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.84 1.80 ug/1 312314 Naphthalene-d8 15.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 59 2 IIH-Dibenzo b,E][1,4]diazepin-ll-on 267 C16H17N3O 013450-73-2 38 3 Benzoic aci< , 2-[(trimethylsilyl)ox 282 C13H22O3Si2 003789-85-3 37 4 Benzoic a cd/ , 2,6-bis[(trimethylsil 370 C16H30O4Si3 Abundance / ..... ~___ 37 003782-85-2 Scan 1067 (14.843 min): 4943.D (-) Th

5000 267 355

■ 45 89 108125 154 177'',?3208223 251 14.60 14.80 15.00 15.20 293 323339 m/z 267.03 42.29% m/z->.. 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyi- 713

355 267 5000 1“^ 14.60 14.80 15.00 15.20 m/z 355.05 37.68% 191207 251 323339 li 'm/2-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #3’7180: 11K-DibeniOtb,E][1,4ldiazepin-l 1-one. 5-(3-aminoprc I 30 118 77 161 267 .......... I\............... 223 14.601£80 1^ 15.20 ' 238 5000 m/z 356.0 14.31%

52 ! ■I Wz->20 Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 7)3 #72300: Benzoic acid, 2-[(trimethylsiiyl)oxy]-, trimethylsi n 14.60 14.80 15.00 15.20__ m/z 268.00 11.87% 267 5000

45 1 , , , j... I 92 ... 7^ 1^1 175 J 93209 2^ 249 J,............ 'm/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15.00 15.20

4943.D GCMS0308.M Tue Apr 02 11:06:55 2002 Page 1

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