GCMS analysis results for sample AE05846, April 23, 2002

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GCMS laboratory report for sample AE05846 analyzed on April 23, 2002, by analyst DLV.

NYC-WTC_000048717–000048736

Folder label: “GCMS X 4/11/02 A 4/15/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR1202\5846.D Vial: 6 Acq On : 15 Apr 2002 12:59 pm Operator: Sample : re-extract Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.83 2.27 ug/1 431193 Naphthalene-d8 15.86 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopent as if oxane, decamethyl- 370 C10H3005Si5 000541-02-6 62 2 Benzeneethana mine, N-[(pentafluorop 475 C21H26F5NO2S12 055429-85-1 43 3 11H-Dibenzo [b ,E][1,4]diazepin-11-on 267 C16H17N3O 013450-73-2 38 4 Benzoic acid. 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 37 Abundance 1 Scan 1065 (14.826 min): 5846.D (-) m/ z 73.00 100.00% 73

5000 267 355 --------- 45 14.40 14.60 14.80 15.00 15.20 I I i 89 108 133 154 177193 223 251 J 293 323339 1 0- — Isossyranire 11 ' r I' *'11 m/z 267.00 40.70% m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.05 37.98% 191207 251 323339 i • ■" i "'i ■ ■ i ■ ■ 1’11111011111111107 ’1’23’0"’’1’32’111*190’-"1’1’11’" p-T m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74573: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.05 14.44% 267 44

mfz-> LX ll, 151 179 209 250 ’’1112111111111121011001701*1120/1-/ —/— 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #37180:11 H-Dibenzo[b,E][1,4]diazepin-11-one, 5-(3-aminopro 30 1 8 14.40 14.60 14.80 15.00 15.20 77 267 m/z 268.00 10.92% 181 223

5000 249

m/z—> 4. 52 I “ ‘11" m | 1 “ * | 1 1 » 1 f i i 11 p ..... 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

5846.D GCMS0412.M Tue Apr 16 15:40:12 2002 Page 2

NYC-WTC_000048725

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NYC-WTC_000048725Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE06429, April 23, 2002 · Box DEP Box 27

NYC-WTC_000048827

GCMS laboratory report for sample AE06429 analyzed on April 23, 2002, by analyst DLV.

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