NYC-WTC_000009619
Calibration table page listing internal standards and response factors for GCMS analysis.
Same agency, volume and box · similarity 0.993
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GCMS calibration analysis results, DEP Labs, Feb 2002
Machine-extracted title · confidence 100%Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
NYC-WTC_000009835–000009850Folder label: “GCMS X 1/22/02 A 2/22/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\FEB2102\472.D Vial: 6 Acq On : 21 Feb 2002 7:01 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
14.93 0.58 ug/1 53721 Naphthalene-d8 15.97
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 86 2 Benzoic acid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 43 3 Phenethylamine, N-met hyl-.bet a. ,3,4 399 C18H37NO3Si3 010538-85-9 32 4 IIH-Dibenzo[b,E][1,4]diazepin-11-on 267 C16H17N3O __ 013450-73-2 27 Abundance 73 Scan 1077 (14.927 min): 472.D (-) | m/z 73.00. 100 .00%
5000 267 355 ----- 45 133 154 177193 . 223 251 323 339 j, 14.60 14.80 15.00 15.20 I Tmmmmmmpm Tp TIIPTTLTRTTTTTTTT m/z 267.00 38.22% m/Z-2.. 40 60 80 100 120 140 160 .180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 I 355 267 5000 14.60 14.80 15.00 15.20 m/z 355.05 34.53% 191207 251 | 323 339 | T‘I—00010011000101021010205211-2001001m011mI ■' i " ' ■ i ‘" i “ ■ 11'1 m/z- 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance 73 +14’’I’ i 1 ■ 1 ■ i ■ ' 1 ■ i 14.60 14.80 15.00 15.20___ 267 5000 m/z 356.0,5 12.04% 45 92 135151 175 193 209 233249 1 ■ । ■ ■ ■ ■ । • 11 ‘ ‘ I T0un]—mmOOuu—Iu[ TT I'1 ■' I' ’' ’ I ’ ‘ m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300320340 360 Abundance #74239: Phenethylamine, N-methyl-beta.,3,4-tris(trimethyis 73 14.60 14.80 15.00 15.20 m/z 268.00 10.67% 5000 355 44
m/z-> ’TI +88 130 147 ‘ I ' “ ' I ' ' ' ‘ I “ ' ‘ I ‘ ‘ ' 1 1 ‘ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 193 ' I ' ' “ I ‘ ‘ 267 294 ‘ I ' ' “ I ' ‘ ‘ ‘ 1 ‘ ' ‘ ' I ' ‘ ‘ I ‘ ‘ ' I ‘ ‘T1 ‘ ' 14.60 14.80 15.00 15.20
472.D GCMS0208.M Fri Feb 22 09:42:11 2002 Page 1
NYC-WTC_000009840
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