GCMS surrogate recovery results, sample AE01137, March 4, 2002

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GCMS results for sample AE01137 showing surrogate recovery data analyzed on March 4, 2002.

NYC-WTC_000009641–000009649

Folder label: “GCMS X 1/14/02 A 3/4/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1137.D Vial: 69 Acq On : 24 Feb 2002 11:59 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.93 0.95 ug/1 83038 Naphthalene-d8 15.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 32 3 Phenethylamine,/N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 32 4 11H-Dibenzo[b,E [l,4]diazepin-ll-on 267 C16H17N3O 013450-73-2 30 Abundance ...................... ’ " I Scan'1077 (14.927 min): 1137.D (-) m/ z 73 .00... 100.00% 73

5000 267 355

. 451 t , 133 154 177 193 223 251 14.60 14.80 15.00 15.20 __ 323 339 I, 1’.’* TTTTumnn—nmumam *dIUaaap*sddITass7—uaTud m/z 267.0,0 39.12% m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 14.60 14.80 15.00 15.20 ' ' m/z 355.05 33.83% 191 207 251 323 339 | n ।ri11.i>।।।।।11111111n111 TI109091ummaagur miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance 21:8ie 3 ■ ! . . !11 dd ( ni ..... .... 73 ’ ’ I * ‘ ' I ' * ’ ‘ I • ‘ ’ I T * ‘ ‘ I’ 14.60 14.80 15.00 15.20 267 5000 179 m/z 356.05 12.10% 356 45 147 209 237 312 341 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance. #74239: Phenethylamine, N-rnethyl-.beta.,3,4-tris(trimethyls 73 __14.60 14.80 15'00 15.20 ‘ m/z 268.0.0 10.94% 5000 355 44 . 88 130 147 193 267 294 | ’ 1 ■11 ■ ■ Tr 11‘' i. ' f. । i ।।।। *}— 1 ' i ■ ‘ ■ i • ■ ■ ■ i ' 1 1 1 I ' 1 1 1 I m/z-> . 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15.00 15.20

1137.D GCMS0208.M Fri Mar 01 09:06:05 2002 Page 2

NYC-WTC_000009648

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