NYC-WTC_000009619
Calibration table page listing internal standards and response factors for GCMS analysis.
Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Document / 16 pages
GCMS calibration analysis results, DEP Labs, Feb 2002
Machine-extracted title · confidence 100%Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
NYC-WTC_000009835–000009850Folder label: “GCMS X 1/22/02 A 2/22/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\FEB21O2\472.D Vial: 6 Acq On : 21 Feb 2002 7:01 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclohexasiloxane, dodecamethy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
18.09 1.01 ug/1 93154 Naphthalene-d8 15.97
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl - 444 C12H3606Si6 000540-97-6 30 2 l,l,l,5,7,7Z7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 3 2H-l,4-Benz6diazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 9 4 Silane, [12,3-benzenetriyltris(oxy 342 C15H30O3Si3 73.00 100.00% 9 017864-23-2 Abundance Scan 1421 (18.085 min): 472.D (-) m/ z 73
5000 341 / 1 147 429
m/z~> 45 , '"i"' i 117 179. 2?7 TunmuugmT] 251 [ mA 295 'i"i ■ 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400 420 L ■ • i" " i' ■' ■ (" r 17.80 m/z 341.00 18.00 18.20 18.40 34.31% Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000 17.80 18.00 18.20 18.40 147 m/z 147.00 14.01% : 117 1 207 267 311 ' i" " i" " i ■" “ "E’TTTTEEIIEIEETTICEIEUUIIUT , Ji, , , , 1 1’—B31—1919——TIE—EI0ITTT v m/z-> .. 40 60 80 100 120140160180200220240 260 280 300320 340360 380400420 Abundance "■ . ........... ........ :.... " 0004 73
147 17.80 18.00 18.20 18.40 5000 267 m/z 342.00 11.10% 355 429 45 207
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance> #48337: 2H-i,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- ........... M........... 73 341 17.80 18.00 18.20 18.40 m/z 325.00 10.78% 5000- 45 91 ,116 146 227 315 269 """ | ■ 11 > ।■ I n j 111111 i rl j 11 ’’0’"u1——"0UEI0’E0—U111UTUTE3"I1T "' i'" ■ i m/Z-? 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400 420 17.80 18.00 18.20 18.40
472 .D GCMS0208.M Fri Feb 22 09:42:15 2002 Page 2
NYC-WTC_000009841
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