GCMS calibration analysis results, DEP Labs, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\472.D Vial: 6 Acq On : 21 Feb 2002 7:01 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanone, 1-(1-methylethoxy Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

18.81 0.46 ug/1 44886 Ac enapht hene-d10 21.29

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1-(1-methylethoxy)- 116 C6H1202 042781-12-4 17 2 Butane/ 58 C4H10 000106-97-8 9 3 2 (1H) -/Pyrimidinone, 4-amino- 111 C4H5N30 000071-30-7 9 4 Imidazole-4 - carboxamide 111 C4H5N3O 000000-00-0 9 Abundance Scan 1500 (18.811 min): 472.D (-) m/z . 42.95.. 100.00% 43 57 73 111 5000 95 I ■ ■ ' 1 I / T 18.40 18.60 18.80 19.00 19.20 .............. 1 ■11 ■ ■ ■ ■ i ■ • ■ ■ i ■ ■ ■ ■ i +, 127 >i ■ 0* 1 11111111 ■ ■ ■ i ■ ■ ■ ■ । 146 m/z 57.00 68.18% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance ' #3286:2-Propanone, 1-(1-methylethoxy)- 43

5000 18.40 18.60 18.80 19.00 19.20 m/z 73.00 63.95%

m/z-> _. 10 20 7. 30 40 58 73 11111''11'11' 1111' 11'11!11 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i1' ■ ■ i ■ ■ ■' i ■ ■ ■ ■ i''

50 60 70 80 90 100 110 120 130 140 150 Abundance 43

18.40 18.60 18.80 19.00 19.20 5000 29 m/z 111.1.0 52.71%

15 58

m/z-> ' 10 20 30 '' 40 "sb " 60 ' 70 80 " 90 100 110 120 130 140 150 Abundance #63896: 2(1H)-Pyrimidinone, 4-amino- 1 1 18.40 18.60 18.80 19.00 19.20 m/z 95.00 33.10% 5000

42 83 55 95 11 11 1' 111 ‘1 ' 11'1 1 P 11 TDTTT ■ ■ i • • ■ ■ i •11' i ■ ■ ■ ■ 1 ' i' • ■ ■ i ■ •'11' ■ ‘ ■ i ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i 1 ■ ■ 1 । ■ 1 ■ ■ i • 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 18.401 18.60 18.80 19.00 19.20

472.D GCMS0208.M Fri Feb 22 09:42:20 2002 Page 3

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