Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
NYC-WTC_000023789–000023810Folder label: “GCMS X 5/9/02 A 5/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\MAY2002\9676.D Vial: 10 Acq On : 20 May 2002 4:02 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 7 2-Propanone, 1-(1-methylethoxy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 18.63 4.36, ug/1 298812 Acenaphthene-dl0 21.08 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2 - Propa: ne, 1-(1-methylethoxy)- 116 C6H1202 042781-12-4 17 2 Butane 58 C4H10 000106-97-8 9 3 2-Pentenoic acid, 4-methyl- 114 C6H10O2 010321-71-8 9 4 2 (5H)-Furanone, 3,5,5-trimethyl - 126 C7H10O2 050598-50-0 9 Abundance Scan 1483 (18.627 min): 9676.D (-) m/z 43.05 100.00% 43 57
5000 73 111 95 18.20 18.40 18.60 18.80 19.00
m/z-> - 4+, ‘rern T 127 85 TTTH T—0010m3T 146 201 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 m/ z 57.10 68.07% Abundance #3286:2-Propanone, 1-(1-methylethoxy)- 43
5000 18.20 18.40 18.60 18.80 19.00 m/ z 73.10 49.60% 27 58 73 11, ''Iil ..... I "'111"11" " । “ i" " i" " i" " r1" i" " i" " r " 11" " I" " 1111111"11'11111"11 " r "11" "i' m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #99: Butane 43 .................. .................... 18.20 18.40 18.60 18.80 19.00 5000 29 m/z 111.20 38.71%
15 58 A m/z-> + m plp I. " " 111" i1 a i ■ ■" i1"' i" " i ‘1" i" " i ■"11'F ■ ■ i ■"111111111111"' 1111111' 11111111111111
10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #2882:2-Pentenoic acid, 4-methyl- ....... ............................... 43 18.20 18.40 18.60 18.80 19.00 m/ Z 41.15 24.53%
5000 59 69 — 114 T’IUIUII" 81 99 I f 1 ) Tin Pi 1 f n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 18.20 18.40 18.60 18.80 19.00
9676.D GCMS0520.M Tue May 21 11:39:19 2002 Page 7
NYC-WTC_000023802
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NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005367
Laboratory report showing non-detectable results for nitrosamines and chlorinated solvents in GCMS blank.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000023646
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000023647
Technical data file header page from a GCMS analysis run associated with the World Trade Center site in May 2002.
Filed in the same folder
NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
Filed in the same folder
NYC-WTC_000023662
Laboratory report showing GC/MS calibration data for volatile organic compounds analyzed on May 20-21, 2002.
Filed in the same folder
NYC-WTC_000023666
Laboratory report showing GC/MS reference analysis for sample AE09676 with quantitative results for volatile organic compounds.
Filed in the same folder