Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
NYC-WTC_000023789–000023810Folder label: “GCMS X 5/9/02 A 5/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2002\9676.D Vial: 10 Acq On : 20 May 2002 4:02 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 8 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 20.74 2.46 ug/1 168868 Acenaphthene-dl0 21.08
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy/l, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 Trisiloxane/ 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 38 3 3-Isopropoxy-1, 1,1,5,5,5-hexamethyl 354 C12H3404Si4 072182-11-7 25 4 4-Amino-5-imidazole carboxamide, tr 342 C13H3 0N4 OS i 3 000000-00-0 7 Abundance Scan 1714 (20.744 min): 9676.D (-) m/z 73.10 100.00%l 73
5000 147 281 ----- 45 20.40 20.60 20.80 21.00 I । ■ 'i ' ' , , ! 117 ,191 221 251 i 327 383 415 ' ' i ■ 1 ' ■ i 1 ' ' ' I ' 1 ■ ' i 1 1 1 1 I 1 ' 1 1 I 1 1 m/Z 147.05 30.82% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 .................. \............ — ‘ ‘ i ' ■ ■ 1 i ■ ■ ' 1 i ' 1 1 1 i ' 1 ■ ■ i ■ 147 20.40 20.60 20.80 21.00 m/Z 281.00 26.74% _ 21 21327 415 519 561 ' ' i ' ' ' ' i ' ' ' ' i ■ ' 1 1 i ' ' ' ' i ■ ' ' ' i ■ ■ ' ' i ■ ' ' 1 i 1 ■ ' ■ i ■ ■ ' 1 I 1 '' 1 1 I 1 1 mz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147
281 20.40 20.60 20.80 21.00 5000 m/z 326.95 8.99%
369 P 27 249 ; 338 | miz-> 50 100 150 200 250 300 350 400 450 500 550 ........... ..... ...... Abundance #49645:3-lsopropoxy-1,1,1,5,5,5-hexamethyl-3-(trimethylsil 73 20.40 20.60 20.80 21.00 281 m/z 74.10 8.81%
5000 207 339
m/z— > ... 133150 177200 1 1 4/11’1 */4/1/1/1/*// 50 100 249, “d/1////1/4/4 250 300 "i IT 350 400 450 500 550 20.40 20.60 20.80 21.00
9676.D GCMS0520.M Tue May 21 11:39:20 2002 Page 8
NYC-WTC_000023803
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NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005367
Laboratory report showing non-detectable results for nitrosamines and chlorinated solvents in GCMS blank.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000023646
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000023647
Technical data file header page from a GCMS analysis run associated with the World Trade Center site in May 2002.
Filed in the same folder
NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
Filed in the same folder
NYC-WTC_000023662
Laboratory report showing GC/MS calibration data for volatile organic compounds analyzed on May 20-21, 2002.
Filed in the same folder
NYC-WTC_000023666
Laboratory report showing GC/MS reference analysis for sample AE09676 with quantitative results for volatile organic compounds.
Filed in the same folder