Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
NYC-WTC_000023789–000023810Folder label: “GCMS X 5/9/02 A 5/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2002\9676.D Vial: 10 Acq On : 20 May 2002 4:02 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 9 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T. 21.50 1.04 ug/1 71028 Acenaphthene-dl0 21.08 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403; 023676-09-7 (95 2 Benzoic acid, 2-hydroxy-, hydrazide 152 C7H8N2O21 000936-02-7 43 Xi 3 l-Cyclopentene-l-propanoic acid, .b 168 C1OH1602: 061833-30-5 38 4 4-Methoxyphenylacetic acid ethyl es 194 C11H1403 014062-18-1 38
3 •undance Scan 1797 (21.504 min): 9676.D (-) 121 m/z 121.05 100.00%!
5000
-H50 , 39 1 65
h 76 # .1 109 93 L 138 149
166 - ‘ I’’ 194 ... a.... 21.20 21.40 21.60 21.80 m/z 149.05 48.62% .13 mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #69400: Benzoic acid, 4-ethoxy-, ethyl ester 121
149 5000 - 194 21.20 21.40 21.60 21.80 65 138 166 m/z 194.10 29.38% 93
m/z-> 30 .............. 50....... i 40 50 60 76... .... .... — 1‘E I 1111111111' " I "1' 11 ‘111 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #10124: Benzoic acid, 2-hydroxy-, hydrazide 121
21.20 21.40 21.60 21.80 5000 m/z 138.10 23.77%| 65 152 93 37 T1mmm1053 I I ——mu—u0IOImOmILuuugTT miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance। #14561:1 -Cyclopentene-1 -propanoic acid, .beta.-methyl-, me 79 121 21.20 21.40 21.60 21.80 58 95 8000 m/z 65.05 21.79% 109 6000 4000 150 ................. .......... ......................................... ............................... A4 m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 21.20 21.40 21.60 21.80
9676.D GCMS0520.M Tue May 21 11:39:21 2002 Page 9
NYC-WTC_000023804
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NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005367
Laboratory report showing non-detectable results for nitrosamines and chlorinated solvents in GCMS blank.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000023646
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000023647
Technical data file header page from a GCMS analysis run associated with the World Trade Center site in May 2002.
Filed in the same folder
NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
Filed in the same folder
NYC-WTC_000023662
Laboratory report showing GC/MS calibration data for volatile organic compounds analyzed on May 20-21, 2002.
Filed in the same folder
NYC-WTC_000023666
Laboratory report showing GC/MS reference analysis for sample AE09676 with quantitative results for volatile organic compounds.
Filed in the same folder