Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
NYC-WTC_000023789–000023810Folder label: “GCMS X 5/9/02 A 5/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2002\9676.D Vial: 10 Acq On : 20 May 2002 4:02 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Cyclohexasiloxane, dodecamethy Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 25.44 1.67 ug/1 101273 Phenanthrene-dl0 25.52
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 32 2 l,l,l,5,7,7/7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 32 3 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 32 4 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 9 Abundance Scan 2226 (25.435 min): 9676.D (-) m/z 73.10 100.00% 73 ft
5000 147 -... r.... 1 m/z-> 45 - ■ ■ i 117 50 100 1 ' ‘ 150 19 1281,325,3554012° m/z 147.05 200 250 300 350 400 450 500 550 25.00 25.20 25.40 25.60 25.80 23 .40% Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 --- 5000 25.00 25.20 25.40 25.60 25.80 147 m/z 221.10 14.14%|
m/z-> 50 ’ I’’ 100 117, 150 200 207 250 267 300 350 1— 400 450 500 550 Abundance #56714:1,1,1,5,7,7t7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 1....... —— i ■ ■ ■ ' i ' ' 147 25.00 25.20 25.40 25.60 25.80 5000 267 m/z 429.05 9.39% 355 429 45 207
m/z- > 50 I ■ ■ । i > —L|...... 1.................................. 100 150 200 1 ' 1 I ' ' f ' I ' 250 300 350 400 ‘ ' I ' 114 I ' ' 450 500 ' ] ' ' ' I I 1 1 1 I I 1 550 Abundance 73 #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim ..................../ I ' ‘ I 1 1 1 1 I 1....... - 25.00 25.20 25.40 25.60 25.80 m/z 74.10 8.50%| 5000 147
221 281 327 1. । 415 519 561 f 1 i 1 1 1 f i 1 1 ’IIIE’II"II1II /z—> 50 100 150 200 250 300 350 400 450 500 550 25.00 25.20 25.40 25.60 25.80
9676.D GCMS0520.M Tue May 21 11:39:22 2002 Page 10
NYC-WTC_000023805
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NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005367
Laboratory report showing non-detectable results for nitrosamines and chlorinated solvents in GCMS blank.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000023646
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000023647
Technical data file header page from a GCMS analysis run associated with the World Trade Center site in May 2002.
Filed in the same folder
NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
Filed in the same folder
NYC-WTC_000023662
Laboratory report showing GC/MS calibration data for volatile organic compounds analyzed on May 20-21, 2002.
Filed in the same folder
NYC-WTC_000023666
Laboratory report showing GC/MS reference analysis for sample AE09676 with quantitative results for volatile organic compounds.
Filed in the same folder