Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
NYC-WTC_000017663–000017674Folder label: “GCMS X 12/13/01 A 12/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\LBA.D Vial: 4 Acq On : 27 Dec 2001 1:06 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.45 0.80 ug/1 279064 Naphthalene-d8 15.29
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 36 2 l,l,l,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 3 Heptadecanoic acid, trimethylsilyl 342 C20H42O2Si 055517-58-3 12 4 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3S13 017864-23-2 10 Abundance Scan 1352 (17.452 min): LBA.D (-) m/z 73.0,0 100.00% 73
5000 341 ‘ 1 ' * | ‘ ‘ ‘ | * . । I | ' ! I 'I I | I I I 147
miz-> mk 45 117 L 1IINTTu 179 . 207 251 281 311 L L 429 .. j.... ।.... । 40 60 80 100120140160180200220240260280300320340360380400420 L . ।. 17.20 17.40 17.60 17.80 m/z 341.00 25.25% Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000 17.20 17.40 17.60 17.80 ‘ 147 m/z 147.op 13.51% ! 117 [ 207 267 311 ।।।।.1..Pi..।...11.1.11।।।। 111111. । >. । ■ 111 ii 11 r. 111 miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714: 1.1,1,5.7.7.7-Heptamethyl-3.3-bis(trimethylsilaxy)t 73 . . p . . । fi i'i । । i i i i । i i 147 17.20 17.40 17.60 17.80 5000 267 m/z 325.00 8.74% 355 429 45 207 I Trrrp-n miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #73597: Heptadecanoic acid, trimethylsilyl ester 73 17.20 17.40 17.60 17.80 m/z 74.00 8.66% 117 « 5000 327 145 I miz-> ‘ ‘I 7.1717497, 201 i.‘i .. p... j.. ।. 11... ।....,.... ।... 111111111111 >
40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
LBA.D GCMS1126.M Wed Jan 02 11:10:27 2002 Page 4
NYC-WTC_000017672
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1 shared topics · Same agency, volume and box · similarity 0.993
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1 shared topics · similarity 0.994
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1 shared topics · similarity 0.993
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1 shared topics · similarity 0.993
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