Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018470–000018491Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30645.D Vial: 53 Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Cyclohexasiloxane, dodecamethy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T. 17.46 8.38 ug/1 204860 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 33 2 1,1,1,5,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 20 3 2H-1,4-B enzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 12 4 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 10 Abundance Scan 1352 (17.457 mln): 30645.D (-) m/z 72.95 100.00% 73
- 5000 341 I I I i [ I I I J ( I N I I * , * I [ — — 147 429 17.20 17.40 17.60 17.80 0-mm 45 L '96gpag 117 I 179 207226 251 281 311 [ [ 367 397 L TMTTTTTTTTTTTUTTDTTTTTT m/z 341.00 37.69% miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 % 341
429 5000 T r1 T T 17.20 17.40 17.60 17,80 147 m/z 147.Q0 15.39% 117 | 207 267 311 .., t.... ।,... ।,... ।.... (.,., ।।..,. ।. 1111 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1.1.1.5,7.7,7-Heptamethyl-3.3-bis(trimethylsiloxy)t 73 ■ • । ■ r■ N ‘ I T 147 17.20 17.40 17.60 17.80 5000 267 m/z 342.00 12.73% 355 429 45 । 207 I TTu j(t... 1j....t।. m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48337:2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- » i i » । « i i i । » i » i j i b b > । i i • 73 341 17.20 17.40 17.60 17.80 m/z 325.00 12.50% 5000 45 91 | 116 146 •»i«। / h 1111 f i j i h 1111 ii । n 111111 i ।1 227mmmE—269 TTn—H— ....—315, uum 1................ ——BOOUEEOIT I i । i > b ( | I »i» । I i i i । < i m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
30645.D GCMS1126.M Fri Feb 01 10:52:46 2002 Page 5
NYC-WTC_000018479
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NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
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NYC-WTC_000018416
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Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
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Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
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Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
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