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GC/MS calibration data for sample 30645, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018470–000018491

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018480
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\30645 .D Vial: 53 Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 2-Propanone, 1-(1-methylethoxy Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

18.15 0.31 ug/1 163098 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1- (1 -methylethoxy) - 116 C6H1202 042781-12-4 23 2 2,4,4-Trintethylbut-2-enolide 126 C7H10O2 004182-41-6 17 3 Furan, trahydro-2,2,5,5-tetrameth 128 C8H160 015045-43-9 10 4 Acetam de, N-methyl- 73 C3H7NO ________ 000079-16-3 9 Abundance * Scan 1428 (18.155 mln): 30645.D (-) m/z 43.00 100.00% 43 57 73 5000 111 95 -PFFTTTP 17.80 18.00 18.20 18.40

m/z-> -44 ‘I’T 85 „ 127136 146 201 I’" ‘ ‘ I rr 111111 |H 111 m'l I n 11111'11111 > 111 n > 111 n |. i. |.... 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 | m/z 57.00 69.93% Abundance #3286:2-Propanone, 1-(1-methylethoxy)- 43

5000 “TTTTTTTmrT 17.80 18.00 18.20 18.40 27 i 58 73 m/z 73.00 53.46% — ‘I’’ "11 TTIIunmuumuuT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150160 170 180 190 200 Abundance #64889: 2.4,4-Trimethylbut-2-enolide 43 TT tor ?= 17.80 18.00 18.20 18.40 5000 111 m/z 111.10 39.33% 83 68 126 mmttSRHp miz-> Abundance> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200

43 #65056: Furan, tetrahydro-2,2,5,5-tetramethyl- m 17.80 18.00 18.20 18.40 m/z 69.10 27.87% 5000 55 113 70 27 95 rp-m-p-m-y h4 ■ I ] l ><. j .... | .'1 j... 4 p ... | . 1.. j || t 1012147 miz-s 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 17.80 18.00 18.20 18.40

30645.D GCMS1126.M Fri Feb 01 10:52:51 2002 Page 6

NYC-WTC_000018480

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NYC-WTC_000018480Source: NYC Law Department, mirrored locally

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