Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018470–000018491Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30645.D Vial: 53 Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 20.28 5.89 ug/1 3145100 Acenaphthene-dl0 20.56 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1,7.7,7-hexamethyl 576 C18H5207Si7 071579-69-6 45 2 Trisiloxane, 1,1,1/5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 3 Phosphoric acid. 3-(ethoxyimino)-2- 429 C14H36NO6PSi3 055334-96-8 10 4 Octadecanoic acid, Abundance 2-[(trimethylsil 386 C22H4603Si_ 056196-58-8 9 Scan 1659 (20.275 min): 30645.D (-) m/ z 73.0.0 100.00% 73
5000 147 281 327 20.00 20.20 20.40 20.60 45 - 18B 117 *9 191 221 251 T*er .. 353,383 415, ' i ■ • ■ ■ i ■ • ' ■ i • ■ m/z 147.00 37.37% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trlm 73
5000 ।: . ri । i i । t । । । 147 20.00 20.20 20.40 20.60 221 281 327 415 519 581 m/z 281.00 34.24% r-. j . . r . । , , . . । . m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane. 1.1.1.5.5,5-hexamethyl-3.3-bis[(trimet 73 147 --- 1 > 1 | I l I l | 1 > >T '| I I ■ 1 | 1 1 I I 281 20.00 20.20 20.40 20.60 5000 m/z 326.90 13.98% 369
miz-> 50 j.. 100 1.207 249 1. 150 200 250 300 338 TIi ' 1 ■ ■ r' ■ ' ■ i ' ‘ 350 400 450 500 550 Abundance #55875: Phosphoric add, 3-(ethoxyimino)-2-[(trimethylsilyl mp* 73 299 20.00 20.20 20.40 20.60 174 328 211 rn/z 282.0.0 9.50% 384 5000 142 357 414 » । » » » i । » । » > । » F » > । » » » t । > t t T" > i » । i i » i । I < । t i i t |- > i i । i • 1 I l , , I ‘ * * ..a m/z-> 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60
30645.D GCMS1126.M Fri Feb 01 10:52:56 2002 Page 7
NYC-WTC_000018481
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NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
Filed in the same folder
NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder