NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30351.D Vial: 20
Acq On : 28 Dec 2001 6:36 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 5 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
20.27 3.72 ug/1 1452490 Acenaphthene-dl0 20.56
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 45
2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37
3 Heptadecanoic acid, trimethylsilyl 342 C20H42O2Si 055517-58-3 9
4 Octadecanoic acid, 2-[(trimethylsil 386 C22H46O3Si 056196-58-8 9
Abundance Scan 1659 (20.273 min): 30351 .D (-) m/ z 73.0,0 100.00%
73
5000
147 281
327 ****** *IIIaITIIII
45 17
117 , 191 221 251 20.00 20.20 20.40 20.60
0- 1 *ii rih Pim T* ..............................
m/z 147.0,0 35.21%
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
73
i •
5000
147 20.00 20.20 20.40 20.60
221 281 327
m/z 281.00 3 0.94%
I ii
415 519 561
m/z—> 50 100 150 200 250 300 350 400 450 500 550’
Abundance #52459: Trisiloxane 1,1,1 5.5,5-hexamrethyi-3.3-bis[(trimet
73 147
281 20.00 20.20 20.40 20.60
5000 m/z 326.90 12.31%
207 ; 389
............................................................................................ ..
miz-> 50 100 150 200 250 300 350 ‘ 400 ' ‘ 450 500 ‘ 550
Abundance #48394: Heptadecanoic acid, trimethylsilyl ester 1 ■ i ' 1 1 ‘ i ■ •
713 20.00 20.20 20.40 20.60
117 m/z 282.00 8.66%
। 5000 327
145
47 201
ha’asnii 1 I ■ 1 ■ 300
■ I • ■ ■ ' i 1 ' 1 1 1 1 1 ' 1 I 1 1 1 1 I ' 1 1 1 I 1 1
- 1 I 1 ■
miz-> 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60
30351.D GCMS1126.M Wed Jan 02 10:46:16 2002 Page 5
NYC-WTC_000017844
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