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GCMS analysis results for sample AD30351, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.

NYC-WTC_000017833–000017853

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document . Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2 701\30351.D Vial: 20 Acq On : 28 Dec 2001 6:36 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 17.45 4.88 ug/1 1711860 Naphthalene-d8 15.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 45 2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19C1N2OSi 055299-24-6 22 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 20 4 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 10 Abundance Scan 1352 (17.455 min): 30351.D (-) m/ z 73.00 1 00.00% 73

5000 341 147 45 429 17.20 17.40 17.60 17.80 miz-> 0-‘T F96.117 [ 179. 207225 251 281 311 L I THTTTTpT TTTTTITTTTr 397 1 m/z 341.00 33.24% 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341

429 5000 17.20 17.40 17.60 17.80 m/z 147.00 14.56% 147 1 ..... ........... ........................................ ................... .. .............. ...................................... ...... m/z-> 40 60 80 100 120 140160180 200220 240 260 280 300 320 340 360 380400420 440 Abundance #48337; 2H-1 4-Benzodiazepin-2-nne, 7-chicro-1.3-dihydro- 5 73 341

17.20 17.40 17.60 17.80 5000 m/z 325.00 11.02% 45 91 । 116 146 227 269 315 TTVI—Ba—m—mmmemmmmemmemgmg mmmmmmpm miz-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t -------- 73 17.20 17.40 17.60 17.80 m/z 429.05 10.80% 147 5000 267 355 429 45 207 TrrqTrrT TIpampng I I *****1414*4*188*81* TIggor .. ।.... । 111 Ai 11 T T T T m/z-> 40 60 80 100120140160180200220240260280300320340360 380 400 420 440 17.20 17.40 17.60 17.80

30351.D GCMS1126.M Wed Jan 02 10:46:11 2002 Page 4

NYC-WTC_000017843

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NYC-WTC_000017843Source: NYC Law Department, mirrored locally

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