Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC2701\30641.D Vial: 42 Acq On : 29 Dec 2001 11:33 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclohexasiloxane, dodecamethy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.45 7.03 ug/1 3757270 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl- 000540-97-6 38 444 C12H3 606Si6 2 1,1,1,5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 27 3 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 4 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 Abundance Scan 1351 (17.448 min): 30641.D (-) m/ z 73.00 100.00% 73
5000- 341 ............ . 147 429 45 , , 97 117 17.20 17.40 17.60 17.80 i [ 179 . 207225 251 281 311 ( | 397 L | 0/’ ’’I’’’ TIUnImmagmumuuuuumagai ■" r ■" i' i m/z 341.00 28.72% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000- 17.20 17.40 17.60 17.80 147 m/z 147.00 14.10% 117 | 207 267 311 1 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance: #56714: 1 . I 1.5.7.7.7-Heptameth-3.3-bis(trimethvisiloxy)t 73
147 17.20 17.40 17.60 17.80 5000 267 m/z 325.00 9.74% 355 429 45 207 -== m/z-> 40 60 80 100120140160180200220240260280300320340 360380400420440 Abundance #48337: 2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 73 341 17.20 17.40 17.60 17.80 m/z 342.00 9.68% 5000 45 91 I 116 146 227 269 315 mpp TTprnTlnTTpT-TTJTTTTp-rTTpT^^ M " ‘ I ‘ nTr " ' ‘ I*'' 'I" "!" m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 17.20 17.40 17.60 17.80
30641.D GCMS1126.M Mon Jan 28 11:13:52 2002 Page 3
NYC-WTC_000004417
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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