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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004418
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30641.D Vial: 42 Acq On : 29 Dec 2001 11:33 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propenenitrile, 3-(acetyloxy Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

18.16 0.39 ug/1 229666 Acenaphthene -dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propenenitrile, 3 - (acetyloxy)- 111 C5H5NO2 014268-54-3 27 2 2(5H)-Furanone, 3,5,5-trimethyl- 126 C7H10O2 050598-50-0 17 3 2-Propanone, 1-(1-methylethoxy)- 116 C6H1202 042781-12-4 16 4 Acetone 58 C3H60 000067-64-1 9 Abundance Scan 1428 (18.155 min): 30641.D (-) m/z 43.05 100.00% I 43 57 73 5000 111 95 —.................... ........... ............. — 17.80 18.00 18.20 18.40

mz-> " r' ■ ■ i" -L-rrpr V 85 ''1 *h i"'11 ....................... 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 I'1 ■ •! 201 " 111" i m/z 56.95 66.31% Abundance #2407: 2-Propenenitrile, 3-(acetyloxy)- i 43 111

5000 — ,.9, ... 17.80 18.00 18.20 18.40 15 77 m/z 73.0.0 59.18% 52 Hm - i'i, 94 । 2mmnnmm*pmmmmg m/z->__ 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 Abundance #4476 2(5)-Furanone. 3 5.5-trimethy- 43 -----

17.80 18.00 18.20 18.40_____ 5000 111 m/z 111.10 45.08% 83 55 68 126

m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200__ Abundance #3286: 2-Propanone, 1-(1-methylethoxy)- 43 17.80 18.00 18.20 18.40 m/z 69.00 26.82% 5000

27 58 73 - "I" "i"" I" II, J .... ' i" " r "1 r " ■ i" " i'" ■ i" ■ ■ i" ■1 r1" i"' ■ r " ■ i" " r " ■ i1"' I" " i 4 m/z-> 10 20 30 40 50 60 70 80 90 100110120 130140150160170 180 190200 17.80 18.00 18.20 18.40

30641.D GCMS1126.M Mon Jan 28 11:13:56 2002 Page 4

NYC-WTC_000004418

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NYC-WTC_000004418Source: NYC Law Department, mirrored locally

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