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GCMS analysis results for sample AD26204, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26204 with unidentified compounds detected.

NYC-WTC_000031129–000031158

Folder label: “GCMS X 11/2/01 A 12/1/01

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Scanned page image, NYC-WTC_000031145
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC0401\26205.D Vial: 68 Acq On : 4 Dec 2001 10:25 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 2-Propenenitrile, 3-(acetyloxy Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 18.17 0.64 ug/l 249057 Acenaphthene-d10 20.59 Hit# of 5 Ten tive ID MW MolForm CAS# Qual --------------------------------------------------- 1 2-Prop e, 3-(acetyloxy)- 111 C5H5NO2 014268-54-3 22 2 Thioph dimethyl- 112 C6H8S 000638-02-8 17 3 Cycloh ---------/e, 4-dimethyl-2-(2-meth 168 C12H24 054411-17-5 12 4 2(1H)- one, 4-amino- 111 C4H5N30 000071-30-7 12 4bundan Scan 1430 (18.175 min): 26205.D (-) m/z 43.05 100.00% - Ah 57 111 yI 95

85 127 146 17.80 18.00 18.20 18.40 18.60 m/z 57.00 71.87 10 20 30 40 50 60 70 80 90 1001101201301401501601701 #2407: 2-Propenenitrile, 3-(acetyloxy)- 111

17.80 18.00 18.20 18.40 18.60 15 77 m/z 73.00 69.22% 2 1 94 _____ 10 20 30 40 50 60 70 80 90 100110120130140150150 1701 #2528: Thiophene, 2,5-dimethyl- 11

97 m/z 111.10 56.11% 59 27 45 85 102030 40 50 60 70 80 90 100110120130140150 16017O1 #68125: Cyclohexane,1,4-dimethyl-2-(2-methylpropyq-, (1.a 11 17.80 18.00 18.20 18.40 18.60 69 m z 95.0.0 32.74%

97 1 70 80 90 10011012( 1801

26205.D NP112601.M The Dec 04 15:58:45 2001 Page 8

NYC-WTC 000031145

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NYC-WTC_000031145Source: NYC Law Department, mirrored locally

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