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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004447
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30707.D Vial: 41 Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Propanone, 1-(1-methylethoxy Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

18.16 0.68 ug/1 399288 Ac enapht hene-d10 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, - (1-methylethoxy)- 116 C6H1202 042781-12-4 17 2 2-Propenenitrile, 3-(acetyloxy)- ill C5H5NO2 014268-54-3 9 3 2-Butanol, 2-nitroso-, acetate (est 145 C6H11NO3 013880-90-5 9 4 Butane ' 58 C4H10 000106-97-8 9 Abundance Scan 1428 (18.157 min): 30707.D (-) m/z 43.0.0 100.00% 43 57 73 5000 111 95

127 146 17.80 18.00 18.20 18.40 111" " I"11111 rln 11 r 1TTTT ,, 85 „ 201 1111 iij'1"।,'1'i■' " r'" i1 ■" i" " i'"11" " i m/z 57.0.0 68.87% m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 Abundance #3286: 2-Propanone, 1-(1-methylethoxy)- I 43 i ........ ..... —

5000 17.80 18.00 18.20 18.40 58 73 m/z 73.0.0 60.18% ...20 In 27 , ' ■ r "' i" " i" ■ ‘i1 m/z—> 10 30 40 50 60 70 80 90 100110120130140150160170180190 200 Abundance 43 #2407- 2-Propenenitrile. 3-(acely oxy) 111 .... n..... 17.80 18.00 18.20 18.40 5000 m/z 111.10 46.99%

15 77 52 i 94 m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 Abundance #8596:2-Butanol, 2-nitroso-, acetate (ester) TTTuurir 43 17.80 18.00 18.20 18.40 m/z 69.10 29.65% 1 5000- 73 27 115 m/z—> mHr - I 56 86 145 1111'1" i111' I''" r "11' ‘" 11'" i" " i" ■' i' ■1 ‘ r'" r ■ ■' i" " i"'' i" " i 10 20 30 40 50 60 70 80 90 100110120130140150 160170 180190200 . . . 17.80 —r । । i r p 18.00 18.20 18.40

30707.D GCMS1126.M Mon Jan 28 11:24:02 2002 Page 5

NYC-WTC_000004447

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NYC-WTC_000004447Source: NYC Law Department, mirrored locally

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