GC/MS calibration data for sample 30647, Dec 2001

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Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\DEC2 701\30706.D Vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Propanone, 1-(1-methylethoxy Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

18.16 0.24 ug/1 135608 Acenaphthene-dl0 20.57

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, I- (1-methylethoxy) - 116 C6H1202 042781-12-4 32 2 Hexanal, ;5 ,B-dimethyl- 128 C8H160 055320-58-6 10 3 Di-tert-butyl peroxide 146 C8H18O2 000110-05-4 10 4 Acetone / 58 C3H60 000067-64-1 9 Abundance Scan 1429 (18.161 min): 30706.D (-) m/z 43.05 100.00% 43 57 73 111 5000 95 TTTPTTDmTTTT 85 127 136 146 17.80 18.00 18.20 18.40 - +15044 ■ l11 I . .'1. ।. +TT T i ■> »'n ■ ■ “ i«»■> ■ i m/z 57.00 66.70% m/z-> 1020 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #3286:2-Propanone, 1-(1-methylethoxy)- 43

5000 om- n4 TFPPPPT 17.80 18.00 18.20 18.40

.. m/z->_____ 10 Abundance l •• 'V 20 30 40 27 + 58 73 1 50 60 70 80 90 100 110 120 130 140 150 #502t Hexanal. 5.5-dimethyl- m/z 73.00 50.99%

57 ! ) 17.80 18.00 18.20 18.40 5000 41 69 m/z 111.10 44.71%

i I 95 i 1. . , 84 441141+14+8114444+4141****1****]/ । ‘ ।' ■ ■ ■ । • i • ■ ■ ■ । TT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #8881: Di-tert-butyl peroxide Tl T IT 57 17.80 18.00 18.20 18.40 m/z 41.05 27.24% 43 5000

15 27 | —1■•।• 11 ■ 73 ! 160311110111 146 TT WAA ‘ l f 1 1 1 1 ’ 1A7T r r m/z-> ■' I ‘ ‘' I' • ‘ ‘ I ‘ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 17.80 18.00 18.20 18.40

30706.D GCMS1126.M Fri Feb 01 11:08:10 2002 Page 5

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