Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018546–000018575Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30706.D Vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 3-Isopropoxy-l, 1,1,7,7,7-hexam Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
20.27 3.35 ug/1 1867950 Acenaphthene-dl0 20.57
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 36 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 3 Octadecanoic acid, 2-[(trimethylsil 386 C22H46O3Si 056196-58-8 9 4 Heptadecanoic acid, trimethylsilyl 342 C20H42Q2Si 055517-58-3 9 Abundance Scan 1659 (20.272 min): 30706.D (-) m/ z 73.0.0 100.00% 73
5000 147 281 45 117 191 2?1 251 t 327 1 355 383 415 20.00 20.20 20.40 20.60 0— TTIn’i eum fi bin Tin m/z 147.00 33.98% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-trls(trim 73
5000 ‘ I***I‘‘1**‘I‘* 1 147 20.00 20.20 20.40 20.60 221 281 327 415 m/z 281.00 30.21% III T11111110n/nnnn—1 /0/nd/nO l —n—mO— OlV 001 STn/6/m/Bd/n/n-d- miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1.1,1,5.5.5-hexamethyl-3,3-bis[(trimet 73 147 • I II DTBEI—G-C2000/m0g//n/8.B 281 20.00 20.20 20.40 20.60 5000 m/z 326.90 12.10% . 369 -
m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52732: Octadecanoic acid, 2-[(trimethylsilyl)oxy}-, methyl 73 20.00 20.20 20.40 20.60 m/z 282.00 8.81% 5000 327 103 371 1 I 129 159
m/z~> * • j 1 50 —p—adal.., M100 150 200 ‘/444144**1**14**‘1*‘‘I****I***}** 250 300 350 400 450 500 550 * ■ ।11 ■ ■ ।! ■ ■' i ■ ■ • ■ । ■ ■ 20.00 20.20 20.40 20.60
30706.D GCMS1126.M Fri Feb 01 11:08:15 2002 Page 6
NYC-WTC_0000 18566
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017782
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD303B5 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
Similarity score 0.998 (not a probability)
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017782
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD303B5 conducted on January 10, 2002.
Similarity score 0.998 (not a probability)
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
Similarity score 0.998 (not a probability)
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
Similarity score 0.998 (not a probability)
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
Similarity score 0.997 (not a probability)
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
Similarity score 0.997 (not a probability)
machine-extracted · confidence unavailable · Check page ↗Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
Filed in the same folder
NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder