GC/MS calibration data for sample 30647, Dec 2001

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Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018546–000018575

Folder label: “GCMS X 12/18/01 A 12/30/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30706.D Vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 3-Isopropoxy-l, 1,1,7,7,7-hexam Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

20.27 3.35 ug/1 1867950 Acenaphthene-dl0 20.57

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 36 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 3 Octadecanoic acid, 2-[(trimethylsil 386 C22H46O3Si 056196-58-8 9 4 Heptadecanoic acid, trimethylsilyl 342 C20H42Q2Si 055517-58-3 9 Abundance Scan 1659 (20.272 min): 30706.D (-) m/ z 73.0.0 100.00% 73

5000 147 281 45 117 191 2?1 251 t 327 1 355 383 415 20.00 20.20 20.40 20.60 0— TTIn’i eum fi bin Tin m/z 147.00 33.98% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-trls(trim 73

5000 ‘ I***I‘‘1**‘I‘* 1 147 20.00 20.20 20.40 20.60 221 281 327 415 m/z 281.00 30.21% III T11111110n/nnnn—1 /0/nd/nO l —n—mO— OlV 001 STn/6/m/Bd/n/n-d- miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1.1,1,5.5.5-hexamethyl-3,3-bis[(trimet 73 147 • I II DTBEI—G-C2000/m0g//n/8.B 281 20.00 20.20 20.40 20.60 5000 m/z 326.90 12.10% . 369 -

m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52732: Octadecanoic acid, 2-[(trimethylsilyl)oxy}-, methyl 73 20.00 20.20 20.40 20.60 m/z 282.00 8.81% 5000 327 103 371 1 I 129 159

m/z~> * • j 1 50 —p—adal.., M100 150 200 ‘/444144**1**14**‘1*‘‘I****I***}** 250 300 350 400 450 500 550 * ■ ।11 ■ ■ ।! ■ ■' i ■ ■ • ■ । ■ ■ 20.00 20.20 20.40 20.60

30706.D GCMS1126.M Fri Feb 01 11:08:15 2002 Page 6

NYC-WTC_0000 18566

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