GCMS analysis results for sample AD30252, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\30252.D Vial: 22 Acq On : 28 Dec 2001 9:31 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

20.27 5.51 ug/1 2501240 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 45 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 33 3 Octadecanoic acid, 2-[(trimethylsil 386 C22H46O3Si 056196-58-8 10 4 Heptadecanoic acid, trimethylsilyl 342 C20H42O2Si 055517-58-3 9 Abundance Scan 1659 (20.271 min): 30252.D (-) m/z 73.00 100.00% 73

5000- 147 281 45 327353 383/15 20.00 20.20 20.40 20.60 — 117 191 191221 -41 249 miz-> 50 I 100 fina irr 150 200 250 Mi m Ti .................................. ■ i ‘ 1 1 • i ■ ■ ' I ■ 1 ■ 1 i ■ ■ ' ■ i 1 ■ • ■ i ‘ ■ 300 350 400 450 500 550 m/z 147.00 35.23% Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 ■ ' ‘ I ‘ ‘ ‘ I ‘ ' r'1 I ‘ ' 1 I ‘ ‘ 147 20.00 20.20 20.40 20.60 221 m/z 281.00 30.72% 2811_____327 L 415 519 561 i 1 1 f 1 i ' 1 1 f i ' ' 1 1 i ‘ 1 ■ ■ i • ■ ■ • i • ■ • ■ i ( ■ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459. Trisiloxane, 1.1.1,5,5.5-hexamethy-3,3-bis[trimet 73 147 281 20.00 20.20 20.40 20.60 5000 m/z 326.90 11.51% 369 ■ ■ । 11 ■ • । 207 249 | ■ i' ‘ 1 • ।1 • • ■ i ‘ । 338 i___________________ ' • ■ i ■ ■ ‘ ■ i 1 ‘ ■ 1 i ' • ■ ■ i ■ ■ ■ • i ■ ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74126: Octadecanoic acid, 2-[(trimethylsilyl)oxy]-, methyl ■ ■ i ■ ■ • • i ’ ‘ • I ■ • ■ • i ■ ■ 73 20.00 20.20 20.40 20.60 327 m/z 282.00 8.77% 5000 371 103129 15g - ' 1 i ’ ■ ■ i k ‘ ‘ ' i ' ' ‘ ■ i ■ ■ ‘ ' i ‘ ' • ■ i ‘ • 1 • i ■ ■ • 1 I ■ • ■ ‘ i ' 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60

30252.D GCMS1126.M Wed Jan 02 10:42:27 2002 Page 6

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