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GCMS analysis results for sample AD31074, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.

NYC-WTC_000017405–000017433

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\31074.D Vial: 12 Acq On 9 Jan 2002 12:04 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 2-Propanone, 1-(1-methylethoxy Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T.

18.00 0.64 ug/1 224918 Acenaphthene-dl0 20.39

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone/1- (1-methylethoxy) - 116 C6H12O2 042781-12-4 25 2 2(5H) -Furanone, 3,5,5-trimethyl- 126 C7H10O2 050598-50-0 23 3 2-Butanol, 2-nitroso-, acetate (est 145 C6H11NO3 013880-90-5 9 4 2-Pent anone 86 C5H10O 000107-87-9 9 Abundance Scan 1412 (18.004 min): 31074.D (-) m/z 43.00 ... 100.00% 43

57 73 5000 111 95 r * ‘ ’’ I ' •! * •11 r * * 17.60 17.80 18.00 18.20 18.40

m/z~> mmm . Hppmt 85 , 127 146 201 TDTTTWTTTTTTTWTTTTNIWTNIWWWTTTWTTTT :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 57.00 65.16% Abundance! #3286: 2-Propanone, 1-(1-methylethoxy)- 43

5000 -PTr 1 i-r 71 m - Pimi 17.60 17.80 18.00 18.20 18.40 m/z 73.00 56.40% 27 58 73 ’"1 .(, ’ , . ,. ।J.. , । .......।।(....j,.,.(....।....j..,....। ■ l" “I ‘ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance 43 1 ■ ’d ‘i -0= r 17.60 17.80 18.00 18.20 18.40 5000 111 m/z 111.10 41.99% 83 55 68 126

miz-s 20 30 40 5o 60 7o 80 90 100 110 120 130 140 150 160 170 180 190 '260 "T ) Abundance #8596:2-Butanol, 2-nitroso-, acetate (ester) 43 17.60 17.80 18.00 18.20 18.40 m/z 69.10 26.92% 5000 73 27 115 -

m/z-> — 56 mm86 Iu—mnmammnm. 145 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 17.60 17.80 18.00 18.20 18.40

31074.D GCMS0103.M Wed Jan 09 12:24:51 2002 Page 9

NYC-WTC_000017421

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NYC-WTC_000017421Source: NYC Law Department, mirrored locally

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