GCMS analysis results for sample AD27288, Jan 2002

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\JAN0802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanone, 1-(1-methylethoxy Concentration Rank II

R.T. EstConc Area Relative to ISTD R.T.

18.01 0.51 ug/1 171766 Acenaphthene-dl0 20.39

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone. 1- (1-methylethoxy) - 116 C6H1202 042781-12-4 32 2 2 (5H) -Furanone, 3,5,5 - trimethyl - 126 C7H10O2 050598-50-0 17 3 Butane / 58 C4H10 000106-97-8 10 4 3-Penten-2-one, 4-methyl-, o-methyl 127 C7H13NO 056336-11-9 9 Abundance Scan 1412 (18.009 min): 27288.D (-) m/z 43.00 100.00%) 43

57 73 5000 111 95 TIT I"fITT 17.60 17.80 18,00 18.20 18.40

miz-> 10 7 TT‘ 111111 20 — 34 .54•i. mfr 85 rrl’i i ■ ...127.... TTur 146 30 40 50 60 70 80 90 100 110 120 130 140 150 m/z 57.00 60.65% Abundance #3286: 2-Propanone, 1-(1-methylethoxy)- 43 - 5000 17.60 17.80 18.00 18.20 18.40 27 , 58 73 m/z 73.00 51.97

m/z-> . . •■1 ti 111 rll . 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 (Abundance #4475: 2(5H)-Furanone, 3.5.5-trimethyl- i 43 ----- / '1 r ■ 17.60 17.80 18.00 18.20 18.40 5000 111 m/z 111.10 41.31 83 55 126 68 ImmPmmpmpmm | ' ■ i'l | । > ri । i‘i > i । i > ■ > । ■ T11—u—mpmpuanum miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #99: Butane 43 17.60 17.80 18.00 18.20 18.40 m/z 69. 24.93 5000 29

15 58

miz-> - 10 20 30 4 50 60 70 80 90 100 110 120 130 140 150 40 TI1II4 1 I 1 1 ' ‘ l 1 1 17.60 17.80 18.00 18.20 18.40

27288.D GCMS0103.M Thu Jan 10 09:36:49 2002 Page 4

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