Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
NYC-WTC_000018005–000018025Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\JAN0802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclohexasiloxane, dodecamethy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.31 4.28 ug/1 1350100 Naphthalene-d8 15.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasilo: .ne, dodecamethyl- 444 C12H36O6Si6 000540-97-6 45 2 2H-1,4-Benzod azepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 3 l,l,l,5,7,7<7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 20 4 Silane, ,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 Abundance Scan 1336 (17.312 min): 27288.D (-) m/z 73.00 100.00%
5000 341 147 TInnnnnm/nm/ 45 , , 96 117 . [ 429 17.00 17.20 17.40 17.60 ___ I IuCmmB — u m— 179 207225 251 281 311. uTTELEuuuT 397 k ’ ’’I’d pTTTpTTTp-rTTJ-r m/z 341.00 3 5.23% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000 17'00 17.20 17.40 17.60 1 147 m/z 147.00 14.21% ______ , 117 [ 207 10mmu—un)Cemm0m—2—m—ua—m——ma3888 267 311 I4481444*1t+1/71/1/141145 ’11322111/1121317 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48337: 2H-1,4-Benzodiazepin-2-one. 7-chtoro-1 3-dihydro-5- 73 341
17.00 17.20 17.40 17.60 5000 m/z 325.00 11.72% 45 | 91 | 116 146 227 269 ’ ’"10041107311 M3lmlmmmmmm7 miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 17.00 17.20 17.40 17.60 m/z 342.00 11.44% 147 5000 267 355 429 45 207 ......... I _ ‘ ‘41’441 TrrrpTTTp-rTTp-rrTTTTTryrrrT[TTT^ Tp]T ■ • i ■ ■ • ■ l 1' ■ i ■ ‘ ■ i ■ • • ■ i m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 17.00 17.20 17.40 17.60
27288.D GCMS0103.M Thu Jan 10 09:36:45 2002 Page 3
NYC-WTC_000018015
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NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017380
Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000017980
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000017981
Laboratory notes regarding GCMS scan results and recovery rates for sample AD25874 dated January 18, 2002.
Filed in the same folder
NYC-WTC_000017989
Gas chromatography-mass spectrometry analysis of sample AD26011 from January 18, 2002, detecting 2-(2-ethoxyethoxy)ethanol and 2-ethoxybutane with no blank contamination.
Filed in the same folder
NYC-WTC_000017997
Laboratory report noting detection of 1,1,2,2-Tetrachloroethane in a water sample with no other non-target compounds.
Filed in the same folder
NYC-WTC_000018026
Laboratory report documenting GCMS analysis of sample AD28968 conducted on January 9, 2002.
Filed in the same folder