Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
NYC-WTC_000018733–000018753Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC3101\30934.D Vial: 51 Acq On 2 Jan 2002 3:21 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 17.46 4.38 ug/1 1379610 Naphthalene-d8 15.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane,/dodecamethyl - 444 C12H3606Si6 000540-97-6 23 2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 12 4 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 Abundance Scan 1352 (17.459 min): 30934.D (-) m/z 73.00 100.00% 73
5000 341 147 J V ' 1 1 ■ i ■ ■ 1 ' 1 1 1T' I 1 1 1 ' 1 1 1 1 45 429 17.20 17.40 17.60 17.80 I 1 99117 179.. 207225 251 281 311L l 1........ 1TDTmmmm 397....... k TrrfrrrrjTT ’001100000001/1003188 m/z 341.00 3 3.80% miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000 ‘ I’’ ‘ ‘ I ' ' 17.20 17.40 17.60 17.80 147 m/z 147.00 14.44% 117 1 207 267 311 . ।.. 111..।.... ।..,. (,, i. (t।. j,.,, ।, 1111.... ।, i., ।.... ।,,.. ।,,,, । r, 11 p 11 > 111111111111 > r 11! 111 40 60 80 100120140160180200220240260280300320340360380400420 (Abundance #48337: 2H-1,4 -Benzodiazepin-2-one. 7-chloro-1.3-dinydro-5- 73 341 nnBBmBBBT/mB/B/Bd/n/n/oon. 17.20 17.40 17.60 17.80 5000 m/z 342.00 11.02% 45 91 i , 116 146 227 269 315 TWmmm—mumammna—mn—mnm—amm—nmnmmupmg mfe-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1,1,1,5,7>7,7-Heptamethyl-3>3-bis(trimethylsiloxy)t 73 17.20 17.40 17.60 17.80 m/z 429.05 10.96% 147 5000 267 355 429 45 207 I I Oupug0uuoa99npmappp Tom9um00-050/50000901——ODROg—t— W- ■ ' i ' • miz-> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
30934.D GCMS1126.M Fri Jan 25 11:46:46 2002 Page 4
NYC-WTC_000018743
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NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
Filed in the same folder