NYC-WTC_000018005
Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 22 pages
GCMS analysis summary, sample AD27288, Dec 2001
Machine-extracted title · confidence 100%GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
NYC-WTC_000016096–000016117Folder label: “GCMS X 12/26/01 A 1/15-1/16/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\JANO 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.31 4.28 ug/1 1350100 Naphthalene-d8 15.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 45 2 2H-1,4-Benzodiazepines-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 3 l,l,l,5,7,7,7-Heptanfethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 20 4 Silane, [1/ 2 * 3 -benzenetriyltris (oxy 342 C15H30O3Si3 017864-23-2 12 Abundance Scan 1336 (17.312 min): 27288.D (-) m/ z 73.00 100.00% 73
5000 341 147 429 45 , 17.00 17.20 17.40 17.60 , 96 117. I I’OBmCIUCTTTTIITITTI ’Tr |........ 397..... k [ 179.207225 251 281 311 L L TTp H 111 n 1111 n ■ | > rt 11 r m/z 341.00 35.23% m/z~> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000 17.00 17.20 17.40 17.60 ' 1 147 m/z 147.00 14.21% 117 | 207 267 311 4 I, TTTTpTTpTTfVpTTTpTTTpTTTyr+TTpTTrpTTTptTTpTTTY^^ ■ i ■ •. • ।“ i •' ■' i ‘■ i1 mz- Abundance 40 60 80 100120140160180200220240260280300320340360380400420 3337; 2H A.Bom 20 : -Ch0rg-1 3- 73 341
17.00 17.20 17.40 17.60 5000 m/z 325.00 11.72% 45 91 i 116 146 227 269 315 • • • > |• 1 ’ •' ‘ I ■ > > । j > 1111 > 11 < । । ।, । > >,, । > 11 > > > > । > 1 > > 11 > < 11 > > i > 11 > < > । ।111 < 1 j > 11111 > > < j > > > > j > > > 111 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyi-3,3-bis(trimethylsiloxyjt 713 17.00 17.20 17.40 17.60 / 1 m/z 342.00 11.44% 147 5000 267 355 429 45 207
mmmmpomH .... j...... I...... TIWIgpr mz-> 40 60 80 100120140160180200220240260280300320340360380400420 ' ' i ■ ■ ■ ■ i ' ' ' ’ i ' • ■ ■ i 1 ' ‘ ■ i 17.00 17.20 17.40 17.60
27288.D GCMS1126.M Mon Feb 04 15:23:03 2002 Page 4
NYC-WTC_000016106
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NYC-WTC_000016106Source: NYC Law Department, mirrored locally
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