Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
NYC-WTC_000018093–000018106Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30694.D Vial: 31 Acq On 1 Jan 2002 6:01 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.45 1.08 ug/1 326040 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 36 2 1,1,1,5, ,7-Heptamethyl -3, 3-bis(t 444 C13H40O5Si6 038147-00-1 25 3 Sila:ne,[1,2,3-benzenetriyltris (oxy 342 C15H30O3Si3 017864-23-2 14 4 2H1 ,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 12 Abundance Scan 1352 (17.454 min): 30694.D (-) m/z 73.0.0 100.00% i 73
5000 341 147 ■ ■ i • ‘ 1’144 45 429 17.20 17.40 17.60 17.80 | 179 207 251 295 323 L - ■ 1... 117TMTTT 11 U1111U (111111A11 r m/z 341.00 28.39% miz-> 40 60 80 100120140160180200220240260280300320340360380400420 (Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341 i
429 5000 ■ ■ i ■ ■ ■ ' i ■ ‘ 17.20 17.40 17.60 17.80 147 m/z 147.00 13.80% I 117 | 207 267 311 l , TImpgu TVmummgDgg" TTp m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714. 1.1,1.5, / .7.7-Heptamethyl-3.3-bis(trimethylsiloxy) 73 ■ • i ■ • 147 17.20 17.40 17.60 17.80 5000 267 m/z 325.00 9.29% 355 429 45 207
miz-> TrpT A ’’l’3’B—91101191010"011B1EU1EPBB291E1T71"1110111101110—SU-1ETCEE0"119""1"17 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48324: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethy- 73 17.20 17.40 17.60 17.80 m/z 74.00 9.12% 239 5000 342
45 133 11I—E1137121177017 __ I 3141. |_________________ । ll., ।,.pl.. p. ।.... j.... ।.... ।..., ।, i" "i • ' i ■ ■ ■ ■ i • ■ ■ • i 1 ■ • ■ i • m!z~> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
30694.D GCMS1126.M Wed Jan 23 08:31:20 2002 Page 4
NYC-WTC_000018103
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NYC-WTC_000018142
Automated laboratory log recording GCMS analysis of sample AD30711 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018650
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018248
Laboratory report documenting GCMS analysis of sample AD30984 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017478
Laboratory report documenting GCMS analysis of sample AD31075 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036815
GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder