Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
NYC-WTC_000018093–000018106Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30694.D Vial: 31 Acq On 1 Jan 2002 6:01 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
14.31 0.89 ug/1 270573 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasilo: e, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 N-(Trifluoroacetyl)-N,O,O',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 47 3 Benzoic d, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40 4 N- (Tri£ uoroacetyl)-0,0*,0'1-tris(t 481 C19H34F3NO4Si3 000000-00-0 38 Abundance (. Scan 1009 (14.306 min): 30694.D (-) m/z 73.00 100.00% 73
5000 267 355 ‘: 45 - 125 154 ,1?3 223 , 323 J ......... 14.00 14.20 14.40 14.60 ' ' ■ ■■■ P 1*/* *ti4 ri m/z 267.00 32.94% miz-> ' 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 %
355 267 5000 14.00 14.20 14.40 14.60 ‘ ‘1 m/z 355.0 22.71% ... ...... 207 ... 323, *I***14/1/4/*/**I4I14III1IS miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacety)-N,0,0,0"-tetrakis(trimethylsi 73
355 14.00 14.20 14.40 14.60 ' 5000 m/z 356.05 8.74%
45 — .147 193... 267....................538 miz-> 50 100 150 200 250 300 350 400 450 500 550 M\ Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet 1 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ • I
73 355 14.00 14.20 14.40 14.60 m/z 74.00 8.57% 5000
147 267
miz-> 47 ‘ ' i ‘ ‘ ' i • • ... .208.237 t . T1 ! J i p ki i J-1 I i t | I i । । | J T" TT—।—r~r 50 100 150 200 250 ’ 300 350 400 450 500 550 14.00 14.20 14.40 14.60 1
30694.D GCMS1126.M Wed Jan 23 08:31:15 2002 Page 3
NYC-WTC_000018102
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NYC-WTC_000018142
Automated laboratory log recording GCMS analysis of sample AD30711 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018650
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018248
Laboratory report documenting GCMS analysis of sample AD30984 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017478
Laboratory report documenting GCMS analysis of sample AD31075 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036815
GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder