Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
NYC-WTC_000018155–000018173Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\DEC3101\30713.D Vial: 28 Acq On 1 Jan 2002 3:07 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.
14.31 2.32 ug/1 816347 Naphthalene-d8 15.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 N-(Trifluoroace 1)-N,0,0',O’’-tetr 553 C22H42F3NO4S14 000000-00-0 43 3 Benzoic acid, 2 ,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40 4 Benzeneeth mine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 38 Abundance Scan 1009 (14.310 min): 30713.D (-) m/z 73.00 100.00% 73
5000 267 355 ‘ ‘ ‘ I ‘ ‘ ‘ I ‘ ‘ • i ‘ ‘ ‘ • I ‘ ‘ 1 I 45 14.00 14.20 14.40 14.60
m/z-> I 99 125 154 * ■ i ’ • • * r ■ • • * । * 50 100 150 —+200293 193 223 250 300 323— 350 400 450 500 550 m/z 267.00 36.08% Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 5000 14.00 14.20 14.40 14.60 m/z 355.05 27.33% ................207 323 j A TIIdon m/z-> 50 100 150 200 * 250 300 350 400 450 500 550 Abundance #60162: N-(Triflucroacety!)-N.0.0,O"-tetrakis(trimethylsi 73 T T 355 14.00 14.20 14.40 14.60 5000 m/z 356.05 9.81%
45 147 193 267 538 50 100 150 200 250 ' '300 i ' 1 ■ • i ‘ ■ 1 i ■ ■ ' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i • • miz-> 350 400 450 500 550 - Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet 73 355 14.00 14.20 14.40 14.60 ' m/z 267.90 9.01% 5000
147 267
m/z-> . ........ 47 50 100 1,111112982376,, 150 200 250 300 1 i n i pi ! i 1 i i n j i i i i । i i r' f j 350 400 450 500 550 T II T 14.00 14.20 14.40 14.60 V TI
30713.D GCMS1126.M Wed Jan 23 08:46:27 2002 Page 3
NYC-WTC_000018164
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NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder